$\require{mediawiki-texvc}$
  • 검색어에 아래의 연산자를 사용하시면 더 정확한 검색결과를 얻을 수 있습니다.
  • 검색연산자
검색연산자 기능 검색시 예
() 우선순위가 가장 높은 연산자 예1) (나노 (기계 | machine))
공백 두 개의 검색어(식)을 모두 포함하고 있는 문서 검색 예1) (나노 기계)
예2) 나노 장영실
| 두 개의 검색어(식) 중 하나 이상 포함하고 있는 문서 검색 예1) (줄기세포 | 면역)
예2) 줄기세포 | 장영실
! NOT 이후에 있는 검색어가 포함된 문서는 제외 예1) (황금 !백금)
예2) !image
* 검색어의 *란에 0개 이상의 임의의 문자가 포함된 문서 검색 예) semi*
"" 따옴표 내의 구문과 완전히 일치하는 문서만 검색 예) "Transform and Quantization"
쳇봇 이모티콘
안녕하세요!
ScienceON 챗봇입니다.
궁금한 것은 저에게 물어봐주세요.

논문 상세정보

Abstract

A high-performance liquid chromatography method was applied to determine the contents of tocopherols in edible oils using a LiChrosorb DIOL HPLC column and hexane fortified with 0.1% acetic acid in an isocratic mode. The validation of the method included tests for linearity, sensitivity, accuracy, precision, and recovery. All calibration curves showed good linear regression ($r^2$>0.9995) within the tested ranges. The established method offered good precision and accuracy with overall intra-day and inter-day variations of 0.94$\sim$4.27 and 1.77$\sim$ 4.88%, respectively. The tocopherol recoveries ranged from 91.44$\sim$108.90%. Subsequently, the method was successfully applied to qualitatively and quantitatively determine the total contents of $\alpha$, $\gamma$, and $\delta$-tocopherols in 12 selected refined edible oils, showing a range of 0.92 to 188.71 mg/100 g.

참고문헌 (23)

  1. Isnardy B, Wagner KH, Elmadfa I. 2003. Effects of ${\alpha},\;{\gamma},\;and\;{\delta}$-tocopherols on the autoxidation of purified rapeseed oil triacylglycerols in a system containing low oxygen. J Agric Food Chem 51: 7775-7780 
  2. Wagner KH, Elmadfa I. 2000. Effects of tocopherols and their mixtures on the oxidative stability of olive oil and linseed oil under heating. Eur J Lipid Sci Technol 102: 624-629 
  3. Jung MY, Min DB. 1990. Effects of ${\alpha},\;{\gamma},\;and\;{\delta}$ -tocopherols on oxidative stability of soybean oil. J Food Sci 55: 1464- 1465 
  4. Satue MT, Huang SW, Frankel EN. 1995. Effect of natural antioxidants in virgin olive oil on oxidative stability of refined, bleached, and deodorized olive oil. J Am Oil Chem Soc 72: 1131-1137 
  5. Nielsen NS, Pedersen A, Sandstrom B, Marckmann P, Hoy CE. 2002. Different effects of diets rich in olive oil, rapeseed oil and sunflower-seed oil on postprandial lipid and lipoprotein concentrations and on lipoprotein oxidation susceptibility. British J Nutr 87: 489-499 
  6. Sotiroudis TG, Kyrtopoulos SA, Xenakis A, Sotiroudis GT. 2003. Chemopreventive potential of minor components of olive oil against cancer. Italian J Food Sci 15: 169-185 
  7. Reiter E, Jiang Q, Christen S. 2007. Anti-inflammatory properties of ${\alpha},\;and\;{\gamma}$ -tocopherol. Mol Aspects Med 28: 668-691 
  8. Junker R, Kratz M, Neufeld M, Erren M, Nofer JR, Schulte H. 2001. Effects of diets containing olive oil, sunflower oil, or rapeseed oil on the hemostatic system. Thromb Haemost 5: 280-286 
  9. Azadmard-Damirchi S, Dutta PC. 2008. Stability of minor lipid components with emphasis on phytosterols during chemical interesterification of a blend of refined olive oil and palm sterin. J Am Oil Chem Soc 85: 13-21 
  10. Gomez-Coronado DJM, Ibanez E, Ruperez FJ, Barbas C. 2004. Tocopherol measurement in edible products of vegetable origin. J Chrom A 1054: 227- 233 
  11. Manan F. 1994. Tocopherol contents of Pakistani seed oils studied by normal phase HPLC. J Islamic Acad Sci 7: 34-38 
  12. Leenheer APD, Lambert WE, Ruyter MGMD. 1992. Modern chromatographic analysis of the vitamins. 3th ed. Marcel Deker, New York, USA. p 160 
  13. Sanchez-Perez A, Delgado-Zamarreno MM, Bustanante- Rangel M, Hernandez-Mendez J. 2000. Automated analysis of vitamin E isomers in vegetable oils by continuous membrane extraction and liquid chromatography-electrochemical detection. J Chrom A 881: 229-241 
  14. Zhang FL, Wei YJ, Zhu J, Gong ZN. 2008. Simultaneous quantitation of three major triterpenoid glycosides in Centella asiatica extracts by high performance liquid chromatography with evaporative light scattering detection. Biomed Chromatogr 22: 119-124 
  15. Sattler SE, Gilliland LU, Magallanes-Lundback M, Pollard M, DellaPenna D. 2004. Vitamin E is essential for seed longevity and for preventing lipid peroxidation during germination. Plant Cell 16: 1419-1432 
  16. Kulas E, Ackman RG. 2001. Different tocopherols and the relationship between two methods for determination of primary oxidation products in fish oil. J Agric Food Chem 49: 1724-1729 
  17. Kiokias S, Vazakas T, Oreopoulou V. 2008. In vitro activity of vitamins, flavonoids, and natural phenolic antioxidants against the oxidative deterioration of oil-based systems. Food Sci Nutr 48: 78-93 
  18. Leckbanda G, Frauena M, Friedt W. 2002. Rapeseed (Brassica napus) breeding for improved human nutrition. Food Res Intl 35: 273-278 
  19. Tuberoso CIG, Kowalczyk A, Sarritzu E, Cabras P. 2007. Determination of antioxidant compounds and antioxidant activity in commercial oilseeds for food use. Food Chem 103: 1494-1501 
  20. Carlucci G, Mazzeo P, Governatore SD, Giacomo GD, Re GD. 2001. Liquid chromatographic method for the analysis of tocopherols in malt sprouts with supercritical fluid extraction. J Chrom A 935: 87-91 
  21. Gliszczynska-Swiglo A, Sikorska E. 2004. Simple reversed- phase liquid chromatography method for determination of tocopherols in edible plant oils. J Chrom A 1048: 195-198 
  22. Kaijeser A, Dutta P, Savage G. 2000. Oxidative stability and lipid composition of macadamia nuts grown in New Zealand. Food Chem 71: 67-70 
  23. Cho EJ, Cho KH, Lee KT. 2005. Lipase-catalyzed synthesis of DHA-enriched structured lipid. Korean J Food Sci Technol 37: 709-712 

이 논문을 인용한 문헌 (1)

  1. Cho, Sung-Hee 2010. "Vitamin E: α-Tocopherol and the Other Forms of Vitamin E" 韓國營養學會誌 = The Korean journal of nutrition., 43(3): 304~314 

원문보기

원문 PDF 다운로드

  • ScienceON :

원문 URL 링크

원문 PDF 파일 및 링크정보가 존재하지 않을 경우 KISTI DDS 시스템에서 제공하는 원문복사서비스를 사용할 수 있습니다. (원문복사서비스 안내 바로 가기)

상세조회 0건 원문조회 0건

DOI 인용 스타일