[논문]Optimization of Oil from Moringa oleifera seed using Soxhlet Extraction method

Ojewumi, M.E.; Oyekunle, D.T.; Emetere, M.E.; Olanipekun, O.O.

doi:10.13106/kjfhc.2019.vol5.no5.11

Optimization of Oil from Moringa oleifera seed using Soxhlet Extraction method 원문보기

The Korean Journal of Food & Health Convergence = 식품보건융합연구, v.5 no.5, 2019년, pp.11 - 25

Ojewumi, M.E. (Chemical Engineering Department, Covenant University) , Oyekunle, D.T. (Chemical Engineering Department, Covenant University) , Emetere, M.E. (Department of Physics, Covenant University) , Olanipekun, O.O. (Chemical Engineering Department, University of Lagos)

Abstract ▼ AI-Helper

Extraction of oil from Moringa oleifera seed using Response Surface Methodology (RSM) was investigated. Effects of three factors namely: sample mass, particle size and extraction time on the response, Moringa oleifera a volume extracted, were determined. The Box-Behnken design of RSM was employed which resulted in 15 experimental runs. Extraction was carried out in a 250 ml Soxhlet extractor with Hexane and Ethanol as solvent. The Moringa oleifera seed powder was packed inside a muslin cloth placed in a thimble of the Soxhlet extractor. The extraction was carried out at 60℃ using thermostatic heating mantle. The solvent in the extracted oil was evaporated and the resulting oil further dried to constant weight in the oven. This study demonstrates that Moringa oleifera oil can be extracted from its seed using ethanol and acetone as extraction solvent. The optimum process variables for both solvent (ethanol and acetone) was determined at sample weight of 40 g, particle size of 325 ㎛ and extraction time of 8 hours. It can be deduced that using acetone as solvent produces a higher yield of oil at the same optimum variable conditions compared to when ethanol was used.

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문제 정의

This study demonstrates that Moringa oleifera oil can be extracted from its seed using ethanol and acetone as extraction solvent. The optimum process variables for both solvent (ethanol and acetone) was determined at sample weight of 40 g, particle size of 325 µm and extraction time of 8 hours.

제안 방법

Experiments were carried out using Box-Behnken response surface design. This require 3 factors with 3 different levels, it resulted into 15 experimental runs.
But it’s cheaper since it requires minimal solvent and minimal effort (Bhutada, 2016). In this study optimization of oil extraction from M. oleifera seeds is carried out in order to determine the best combination of variables required for obtaining the optimum oil yield.
9966 was determined using acetone as extraction solvent. These study validate the effectiveness of using RSM model as a good predictive optimization tool for the extraction of oil from Moringa oleifera seeds using ethanol and acetone as solvent.

이론/모형

The essence of the regression model was determined by F and P values using test for Fischer’s and null-hypothesis.
This was carried out using (Ojewumi, 2018d) method.
This was carried out using (Ojewumi, Adedokun, Omodara, et al., (2017c); Ojewumi, Banjo, Oresegun, et al., 2017d;Ojewumi, Adedokun, Ayoola, & Taiwo, 2018d) method.

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