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특허 상세정보

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Catalytic method for the preparation of lignin phenol surfactants in organic solvents

특허상세정보
국가/구분 United States(US) Patent 등록
국제특허분류(IPC7판) C07G-001/00    C08L-097/00   
미국특허분류(USC) 53/0502 ; 53/050.6
출원번호 US-0082812 (1998-05-21)
발명자 / 주소
출원인 / 주소
대리인 / 주소
    Delhommer
인용정보 피인용 횟수 : 23  인용 특허 : 14
초록

A method of making surfactants from lignin is disclosed by reducing lignin in the presence of a metal oxide or iron based catalyst in an organic hydrogen donor solvent to produce lignin phenol and subjecting the lignin phenol to one or a combination of several reactions such as alkoxylation, alkylation, sulfonation, sulfation, alkoxysulfation, and sulfomethylation. The lignin surfactants so produced can be employed in a surfactant system to recover oil from underground formations.

대표
청구항
▼

[ What is claimed is:] [1.] A method of producing lignin phenol from lignin, the method comprising:placing lignin in contact with a hydrogen donor organic solvent;converting the lignin into low molecular weight-lignin phenol by reducing the lignin in the presence of a reducing agent and a catalyst at a temperature of at least about 200.degree. C. and a pressure of at least about 100 psig;wherein said catalyst contains from about 1.0% to about 15% by weight molybdenum oxide and a second component selected from the group consisting of nickel oxide or cobal...

이 특허에 인용된 특허 (14)

  1. Naae Douglas G. (Houston TX) Davis Centha A. (Houston TX). Enhance oil recovery using oil soluble sulfonate surfactants from lignin and alkylphenol. USP1992035095985.
  2. Morrow Lawrence R. (Richmond TX). Enhanced oil recovery using alkylated, sulfonated, oxidized lignin surfactants. USP1992035094295.
  3. Naae Douglas G. (Houston TX) Davis Centha A. (Houston TX). Enhanced oil recovery using oil soluble sulfonates from lignin and benzyl alcohol. USP1992035095986.
  4. Debons Francis E. (Richmond TX). High salinity polymer drive for surfactant flooding systems. USP1989044821803.
  5. Naae Douglas G. (Houston TX) DaGue Michael G. (Houston TX) Dunn Nancy G. (Houston TX). Hydrocarbon recovery comprising injecting a slug comprising oil soluble alkoxylated surfactants from lignin. USP1993075230814.
  6. Engel Dusan J. (Des Plaines IL) Steigleder Karl Z. (Glen Ellyn IL). Hydrocracking process for liquefaction of lignin. USP1987034647704.
  7. Dai Pei-Shing E. (Port Arthur TX) Sherwood ; Jr. David E. (Beaumont TX) Petty Randall Hughes (Port Neches TX). Hydrodesulfurization of cracked naphtha with hydrotalcite-containing catalyst. USP1994085340466.
  8. Dai Eugene Pei-Shing (Port Arthur TX) Sherwood ; Jr. David E. (Beaumont TX). Hydrodesulfurization of cracked naphtha with low levels of olefin saturation. USP1994105358633.
  9. Dai Eugene P.-S. (Port Arthur TX) Sherwood ; Jr. David E. (Beaumont TX) Martin Bobby R. (Beaumont TX) Petty Randall H. (Port Neches TX). Hydrodesulfurization process. USP1995085441630.
  10. Dai Pei-Shing E. (Port Arthur TX) Sherwood ; Jr. David E. (Beaumont TX) Petty Randall H. (Port Neches TX). Hydrotalcite-containing catalyst composition. USP1995105459118.
  11. Kieke, Dan E.; Naae, Douglas G.. Lignin phenol/lignin/amine surfactant system. USP1991075035288.
  12. Urban Peter (Northbrook IL) Engel Dusan J. (Des Plaines IL). Process for liquefaction of lignin. USP1988034731491.
  13. Naae Douglas G. (Houston TX) Whittington Lawrence E. (Katy TX) Ledoux Will A. (Sugar Lane TX) Debons Francis E. (Richmond TX). Recovering hydrocarbons with surfactants from lignin. USP1988114787454.
  14. Naae Douglas G. (Houston TX) Whittington Lawrence E. (Katy TX) Ledoux Will A. (Sugar Lane TX) Debons Francis E. (Richmond TX). Surfactants from lignin. USP1988044739040.

이 특허를 인용한 특허 피인용횟수: 23

  1. Gray, Lon Montgomery; Scheibel, Jeffrey John; Vinson, Phillip Kyle; Binski, Christopher James. Alkyl-capped alkoxylated esters and compositions comprising same. USP2010027662982.
  2. Gray, Lon Montgomery; Scheibel, Jeffrey John; Vinson, Phillip Kyle; Binski, Christopher James. Alkyl-capped alkoxylated esters and compositions comprising same. USP2012038143208.
  3. Gray, Lon Montgomery; Scheibel, Jeffrey John; Vinson, Phillip Kyle; Binski, Christopher James. Alkyl-capped alkoxylated esters and compositions comprising same. USP2005026849751.
  4. Gray,Lon Montgomery; Scheibel,Jeffrey John; Vinson,Phillip Kyle; Binski,Christopher James. Alkyl-capped alkoxylated esters and compositions comprising same. USP2006077081541.
  5. Massey-Brooker, Anju Deepali; Vaccaro, Mauro; Scialla, Stefano; Crestini, Claudia; Lange, Heiko. Consumer goods product comprising functionalised lignin oligomer. USP2018029895445.
  6. Massey-Brooker, Anju Deepali; Vaccaro, Mauro; Scialla, Stefano; Crestini, Claudia; Lange, Heiko. Consumer goods product comprising functionalised lignin oligomer. USP2018029902812.
  7. Massey-Brooker, Anju Deepali; Vaccaro, Mauro; Scialla, Stefano; Crestini, Claudia; Lange, Heiko. Consumer goods product comprising functionalised lignin oligomer. USP2018039907742.
  8. Massey-Brooker, Anju Deepali; Vaccaro, Mauro; Scialla, Stefano; Crestini, Claudia; Lange, Heiko. Consumer goods product comprising functionalised lignin oligomer. USP2018029901526.
  9. Massey-Brooker, Anju Deepali; Vaccaro, Mauro; Scialla, Stefano; Benjelloun-Mlayah, Bouchra; Crestini, Claudia; Lange, Heiko. Consumer goods product comprising lignin oligomer. USP2018039907744.
  10. Dhepe, Paresh Laxmikant; Kutteri, Deepa Ayillath. Depolymerization of lignin using solid acid catalysts. USP2015069051244.
  11. McCall, Michael J.; Allen, Robert J.; Mackowiak, David E.. Enhancing conversion of lignocellulosic biomass. USP2011098013195.
  12. Scheibel, Jeffrey John. Household cleaning and/or laundry detergent compositions comprising lignin-derived materials. USP2004026689737.
  13. Ling, Tien-Feng; Liu, Zhaoqing; Bottorff, Kyle J. Methods for inhibiting the deposition of organic contaminates in pulp and papermaking systems. USP20190410253214.
  14. Dhepe, Paresh Laxmikant; Sahu, Ramakanta. One pot and single step hydrolytic process for the conversion of lignocellulose into value added chemicals. USP2016029267181.
  15. Schinski, William Lawrence; Kuperman, Alexander E.; Han, Jinyi; Naae, Douglas Gene. Process for generating a hydrocarbon feedstock from lignin. USP2014088795472.
  16. Schinski, William Lawrence; Kuperman, Alexander E.; Han, Jinyi; Naae, Douglas Gene. Process for generating a hydrocarbon feedstock lignin. USP2014118894818.
  17. Chheda, Juben Nemchand; Van Der Heide, Evert. Process for the production of alcohols from biomass. USP2013128609379.
  18. Powell, Joseph Broun; Chheda, Juben Nemchand. Process to produce biofuels from biomass. USP2017039587179.
  19. Powell, Joseph Broun; Chheda, Juben Nemchand. Process to produce biofuels from biomass. USP2015089102878.
  20. Powell, Joseph Broun; Chheda, Juben Nemchand. Process to produce biofuels from biomass. USP2016079394485.
  21. Powell, Joseph Broun; Chheda, Juben Nemchand. Process to produce biofuels from biomass. USP2014048692041.
  22. Powell, Joseph Broun; Chheda, Juben Nemchand. Process to produce biofuels from biomass. USP2015129222028.
  23. McCall, Michael J.. Production of chemicals from pyrolysis oil. USP2012048158842.

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