초록 ▼

Hexabenzylhexaazaisowurtzitane is converted to tetracetyl, dibenzyl azaisowurtzitane. The benzyl groups are removed by catalytic transfer hydrogenolysis leaving a pair of available nitrogens. The available nitrogens are acetylated, and the resulting intermediate is converted to CL-20 with a strong n

Hexabenzylhexaazaisowurtzitane is converted to tetracetyl, dibenzyl azaisowurtzitane. The benzyl groups are removed by catalytic transfer hydrogenolysis leaving a pair of available nitrogens. The available nitrogens are acetylated, and the resulting intermediate is converted to CL-20 with a strong nitrating agent.

대표청구항 ▼

[ What is claimed is:] [1.] A method of preparing an energetic compound having the formula II: [ STR 22 ] comprising nitrating a compound having the formula VI: [ STR 23 ] wherein R is selected from the group consisting of alkyl, cycloalkyl, aryl, arylalkyl, alkene, alkyne, substituted forms of any

[ What is claimed is:] [1.] A method of preparing an energetic compound having the formula II: [ STR 22 ] comprising nitrating a compound having the formula VI: [ STR 23 ] wherein R is selected from the group consisting of alkyl, cycloalkyl, aryl, arylalkyl, alkene, alkyne, substituted forms of any of these groups and H, with a strong nitrating agent.