Method for treatment of surfaces with ultraviolet light
IPC분류정보
국가/구분
United States(US) Patent
등록
국제특허분류(IPC7판)
C08F-002/46
C08J-007/18
출원번호
US-0287978
(1999-04-07)
발명자
/ 주소
Drzal, Lawrence T.
Dontula, Narasimharao
Schalek, Richard L.
Bhurke, Alekh S.
Rich, Michael J.
Fisher, Laura M.
Xie, Ming
출원인 / 주소
Board of Trustees of Michigan State University
대리인 / 주소
McLeod, Ian C.
인용정보
피인용 횟수 :
17인용 특허 :
13
초록▼
A method using irradiation with optical light having a wavelength of 160 to 500 nanometers without higher wavelengths with cooling of the surface during the irradiation to modify the surface (12A, 104A, 202A, 304A, 402A, 502A) of a substrate (12, 104, 202, 304, 402, 502) is described. The light is f
A method using irradiation with optical light having a wavelength of 160 to 500 nanometers without higher wavelengths with cooling of the surface during the irradiation to modify the surface (12A, 104A, 202A, 304A, 402A, 502A) of a substrate (12, 104, 202, 304, 402, 502) is described. The light is filtered or the lamp (24, 106, 212, 306, 510) is restricted to the limited range to avoid the affects of the higher spectra. The light can be pulsed or continuous. The method is significantly enhanced by the presence of water (14, 124, 204, 306, 410, 508) on the surface, preferably also in the presence of ozone in the water. The treated surfaces are more paintable and bondable.
대표청구항▼
A method using irradiation with optical light having a wavelength of 160 to 500 nanometers without higher wavelengths with cooling of the surface during the irradiation to modify the surface (12A, 104A, 202A, 304A, 402A, 502A) of a substrate (12, 104, 202, 304, 402, 502) is described. The light is f
A method using irradiation with optical light having a wavelength of 160 to 500 nanometers without higher wavelengths with cooling of the surface during the irradiation to modify the surface (12A, 104A, 202A, 304A, 402A, 502A) of a substrate (12, 104, 202, 304, 402, 502) is described. The light is filtered or the lamp (24, 106, 212, 306, 510) is restricted to the limited range to avoid the affects of the higher spectra. The light can be pulsed or continuous. The method is significantly enhanced by the presence of water (14, 124, 204, 306, 410, 508) on the surface, preferably also in the presence of ozone in the water. The treated surfaces are more paintable and bondable. arbon compound comprising a hydroxyl-substituted polymer of a diene; (b) mixing the resulting coated rubber particles with a bonding material; (c) spreading the resulting mixture on a substrate; and, (d) allowing and/or causing the resulting mixture to form the desired coherent rubber composition. 15. A coherent rubber composition that has been obtained by the process of claim 14. 16. A coherent rubber composition according to claim 15, in the form of a laid play surface or sports surface. 17. A coherent rubber composition according to claim 15, in the form of a mat, sheet or other moulded article. m and said film having a higher film strength than a film of lesser thickness, wherein said composition further comprises at least one plasticizing agent in an amount ranging from 3 wt. % to 9 wt. % of said composition and at least one acidic stabilizing agent having a pKaof from about 1 to about 5. 3. A method according to claim 1, wherein more than one application of said adhesive composition is provided across said abutted tissue surfaces. 4. A method according to claim 3, wherein said adhesive composition applied across said abutted tissue surfaces is allowed to at least partially polymerize prior to subsequent coatings or applications of said adhesive composition. 5. A method according to claim 3, wherein an adhesive composition having a monomer different from the monomer of a previous coating is applied as a subsequent coating. 6. A method according to claim 1, wherein said adhesive composition polymerizes to form a bridge across said abutted tissue surfaces. 7. A method according to claim 1, wherein said film has a thickness of 0.2 mm to 3.0 mm. 8. A method according to claim 1, wherein said adhesive composition is applied using a crushable swab applicator. 9. The method of claim 1, wherein said adhesive composition comprises at least one plasticizing agent present in the composition in an amount of from 0.5 wt. % to 16 wt. % of the composition; and at least one acidic stabilizing agent having a pKaionization constant of from about 0 to about 7. 10. A film formed across abutted tissue surfaces made by the method of claim 2. 11. A method of forming a biocompatible film across abutted tissue surfaces of an incision or laceration, comprising (a) holding together at least two tissue surfaces of an incision or laceration to form abutted tissue surfaces, (b) applying across said abutted tissue surfaces a sterile adhesive biocompatible monomer composition comprising at least one α-cyanoacrylate monomer, and (c) allowing components of said composition to polymerize and form a biocompatible film on said abutted tissue surfaces having a film strength of at least 70 mmHg of pressure required to induce wound failure and said film having a thickness of at least 0.1 mm. 12. A method according to claim 11, wherein said film strength is at least 90 mmHg of pressure required to induce wound failure. 13. A method according to claim 11, wherein said film strength is at least 100 mmHg of pressure required to induce wound failure. 14. The method according to claim 2, wherein said at least one plasticizing agent is present in an amount of from 4 wt. % to 7 wt. % of the composition. 15. The method of claim 11, wherein said α-cyanoacrylate is selected from the group consisting of 2-octyl cyanoacrylate, dodecyl cyanoacrylate, 2-ethylhexyl cyanoacrylate, butyl cyanoacrylate, methyl cyanoacrylate, 3-methoxybutyl cyanoacrylate, 2-butoxyethyl cyanoacrylate, 2-isopropoxyethyl cyanoacrylate, and 1-methoxy-2-propyl cyanoacrylate. 16. The method of claim 1, wherein said α-cyanoacrylate is selected from the group consisting of 2-octyl cyanoacrylate, dodecyl cyanoacrylate, 2-ethylhexyl cyanoacrylate, butyl cyanoacrylate, methyl cyanoacrylate, 3-methoxybutyl cyanoacrylate, 2-butoxyethyl cyanoacrylate, 2-isopropoxyethyl cyanoacrylate, and 1-methoxy-2-propyl cyanoacrylate. 17. A method of joining together living tissue surfaces of an incision or a laceration, comprising: holding together, without adhesives, at least two tissue surfaces of an incision or a laceration to form abutted tissue surfaces; applying across said abutted tissue surfaces a film of a sterile adhesive composition comprising at least one α-cyanoacrylate monomer; and allowing said composition to polymerize in a film at least 0.1 mm thick, said film having a higher strength than a film of lesser thickness. 18. A method of joining together living tissue surfaces of an incision or a laceration, comprising: (a) holding together at least two tissue
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