초록

The present invention relates to a heated capillary assembly which connects an atmospheric pressure ionization source to a lower pressure mass analyzing system which comprises a capillary tube removably secured to, and extending through the bore of a capillary support assembly.

대표청구항 ▼

1. A mass spectrometer system comprising an ionization chamber and a lower pressure mass spectrometer system and a capillary tube assembly coupling said ionization chamber to said lower pressure mass spectrometer system to allow ions and gas to flow from the ionization chamber into the mass spectrom

1. A mass spectrometer system comprising an ionization chamber and a lower pressure mass spectrometer system and a capillary tube assembly coupling said ionization chamber to said lower pressure mass spectrometer system to allow ions and gas to flow from the ionization chamber into the mass spectrometer system, characterized in that said capillary tube assembly includes: a support assembly having an axial bore, a capillary tube extending through said axial bore and removable from the support assembly, and a securing assembly for sealably engaging and securing one end of said capillary tube to one end of the support assembly. 2. A mass spectrometer system as in claim 1 in which the support assembly is a heated support assembly. 3. A mass spectrometer system as in claim 1 in which the capillary tube is directly heated by passage of electrical current therealong. 4. A mass spectrometer system as in claim 1, 2 or 3 including means for inhibiting venting of said lower pressure mass spectrometer system when the capillary is removed from the support assembly bore. 5. A heated capillary tube assembly for connecting an ionization chamber to a lower pressure chamber in a mass analyzing system comprising: a heated support assembly having an axial bore, a capillary tube extending through said axial bore and removable from the heated assembly, and a securing assembly for sealably engaging and securing one end of the capillary tube to one end of the heated support assembly. 6. A heated capillary tube assembly as in claim 5 including means for restricting the flow of gases through the bore of the heated support assembly from the ionization chamber to the lower pressure chamber when the capillary tube is removed. 7. A heated capillary tube assembly as in claim 6 in which said restricting means comprises a flap mounted on the other end of the heated support assembly. 8. A heated capillary tube assembly as in claim 6 in which said restricting means comprises a ball which falls into said heated support assembly bore when the capillary tube is removed. 9. A heated capillary tube assembly as in claim 5 in which said securing assembly comprises a nut threadably received by the one end of the heated support assembly. 10. A heated capillary tube assembly as in claim 9 including a sealing member between said nut and said heater assembly which is compressed against the capillary tube and heated support assembly when the nut is tightened. 11. A heated capillary tube assembly as in claim 10 in which said sealing member is a ferrule. 12. A heated capillary tube assembly as in claim 9 including an o-ring disposed between the nut and the one end of the heater assembly which is compressed against the heated support assembly and capillary tube when said nut is tightened to form a seal. 13. A mass spectrometer system as in claim 1 in which the support assembly and the capillary tube are electrically connected. 14. A heated capillary tube assembly as in claim 5 in which the support assembly and the capillary tube are electrically connected. 15. A mass spectrometer system as in claim 1, further comprising a spring assembly which presses the capillary tube against the support assembly. 16. A heated capillary tube assembly as in claim 5, further comprising a spring assembly which presses the capillary tube against the support assembly.