IPC분류정보
국가/구분 |
United States(US) Patent
등록
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국제특허분류(IPC7판) |
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출원번호 |
US-0980361
(2004-11-03)
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발명자
/ 주소 |
- Chauhan,Satya P.
- Samuels,William D.
- Kuczek,Sara F.
- Conkle,H. Nicholas
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출원인 / 주소 |
- Battelle Memorial Institute
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대리인 / 주소 |
MacMillan, Sobanski, Todd, LLC
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인용정보 |
피인용 횟수 :
4 인용 특허 :
22 |
초록
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In a process for producing a deicing/anti-icing fluid, a byproduct stream is obtained from a process that produces monoalkyl esters of long chain fatty acids. The stream includes water, glycerol, and an alkali-containing compound. The stream is converted to a deicing/anti-icing fluid by adding an ac
In a process for producing a deicing/anti-icing fluid, a byproduct stream is obtained from a process that produces monoalkyl esters of long chain fatty acids. The stream includes water, glycerol, and an alkali-containing compound. The stream is converted to a deicing/anti-icing fluid by adding an acid to the stream to neutralize the alkali-containing compound to produce an alkali salt that functions as a supplemental freezing point depressant.
대표청구항
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What is claimed is: 1. A process for producing a deicing/anti-icing fluid comprising: obtaining a byproduct stream from a process that produces alkyl esters, the stream including water, glycerol, and an alkali-containing compound; and converting the stream to a deicing/anti-icing fluid by adding an
What is claimed is: 1. A process for producing a deicing/anti-icing fluid comprising: obtaining a byproduct stream from a process that produces alkyl esters, the stream including water, glycerol, and an alkali-containing compound; and converting the stream to a deicing/anti-icing fluid by adding an acid to the stream to neutralize the alkali-containing compound to produce an alkali salt that functions as a supplemental freezing point depressant. 2. A process according to claim 1 wherein the alkali-containing compound is a catalyst in the process that produces the alkyl esters. 3. A process according to claim 1 wherein the alkali-containing compound is selected from the group consisting of alkali metal hydroxides, alkali metal alkoxides, and combinations thereof. 4. A process according to claim 1 wherein the alkali salt is selected from the group consisting of alkali acetates, alkali succinates, alkali phosphates, alkali chlorides, and combinations thereof. 5. A process according to claim 1 wherein the byproduct stream additionally includes a material selected from the group consisting of alcohols, free fatty acids, and combinations thereof, and wherein the process comprises an additional step of removing at least a portion of the material from the stream. 6. A process according to claim 1 comprising an additional step of adding to the stream a material selected from the group consisting of corrosion inhibitors, pH adjusters and/or buffers, emulsifiers, additional freezing point depressants, preservatives, colorants, wetting agents, and combinations thereof. 7. A process according to claim 1 wherein the acid is not a strong acid. 8. A process according to claim 1 wherein the alkali salt additionally includes an alkali acetate, an alkali succinate, an alkali chloride, or a combination thereof. 9. A process according to claim 1 wherein the alkali salt comprises an alkali acetate, and wherein the total amount of the alkali acetate is from 2% to 40% by weight of the fluid. 10. A process according to claim 1 wherein the alkali salt comprises an alkali succinate, and wherein the total amount of the alkali succinate is from 2% to 10% by weight of the fluid. 11. A process according to claim 1 wherein the byproduct stream is obtained from a process that produces monoalkyl esters of long chain fatty acids. 12. A process according to claim 11 wherein the process that produces monoalkyl esters of long chain fatty acids is a process for esterifying a triglyceride. 13. A process according to claim 11 wherein the byproduct stream additionally includes a material selected from the group consisting of alcohols, free fatty acids, and combinations thereof, and wherein the process comprises an additional step of removing at least a portion of the material from the stream. 14. A process according to claim 11 comprising an additional step of adding to the stream a material selected from the group consisting of corrosion inhibitors, pH adjusters and/or buffers, emulsifiers, additional freezing point depressants, preservatives, colorants, wetting agents, and combinations thereof. 15. A process according to claim 11 wherein the alkali salt includes an alkali phosphate in an amount within a range of from about 0. 05% to about 1% by weight of the deicing/anti-icing fluid. 16. A process according to claim 11 wherein the alkali salt functions as both a buffer and a freezing point depressant. 17. A process according to claim 11 wherein the fluid does not contain alkali sulfates or alkali nitrates. 18. A process according to claim 11 wherein the alkali salt has low corrosion properties such that it is not deleterious to metals, roadways or concrete. 19. A process for producing a deicing/anti-icing fluid comprising: obtaining a byproduct stream from a process that produces alkyl esters, the stream including water, glycerol, free fatty acids, and an alkali-containing compound; and converting the stream to a deicing/anti-icing fluid by adding an acid to the stream to neutralize the alkali-containing compound to produce an alkali salt that functions as a supplemental freezing point depressant; and removing the free fatty acids from the fluid. 20. A process according to claim 19 wherein the removal of the free fatty acids is facilitated by adding a material to the fluid to increase its bulk density before removing the free fatty acids. 21. A process according to claim 19 wherein the acid is not hydrochloric acid. 22. A process according to claim 19 wherein the acid is not a strong acid. 23. A process according to claim 19 wherein the fluid meets the requirements of AMS 1435A specification for a runway deicing/anti-icing fluid. 24. A process according to claim 19 wherein the fluid meets the requirements of AMS 1424E specification for an aircraft deicing/anti-icing fluid. 25. A process according to claim 19 wherein the byproduct stream further includes esters, and wherein the process further includes a step of removing the esters from the fluid. 26. A process according to claim 19 wherein the byproduct stream further includes color bodies, and wherein the process further includes a step of removing the color bodies from the fluid. 27. A process according to claim 19 wherein the byproduct stream further includes odorous materials, and wherein the process further includes a step of removing the odorous materials from the fluid. 28. A process according to claim 19 wherein the alkali-containing compound is selected from the group consisting of alkali metal hydroxides, alkali metal alkoxides, and combinations thereof. 29. A process according to claim 19 wherein the alkali salt is selected from the group consisting of alkali acetates, alkali succinates, alkali phosphates, alkali chlorides, and combinations thereof. 30. A process according to claim 19 wherein the byproduct stream is obtained from a process that produces monoalkyl esters of long chain fatty acids. 31. A process according to claim 30 wherein the process that produces monoalkyl esters of long chain fatty acids is a process for esterifying a triglyceride. 32. A process according to claim 19 wherein the alkali salt includes an alkali phosphate in an amount within a range of from about 0. 05% to about 1% by weight of the deicing/anti-icing fluid. 33. A process according to claim 19 wherein the alkali salt functions as both a buffer and a freezing point depressant. 34. A process for producing a deicing solid having reduced corrosiveness comprising: obtaining a byproduct stream from a process that produces alkyl esters, the stream including water, glycerol, and an alkali-containing compound; converting the stream to a deicing/anti-icing fluid by adding an acid to the stream to neutralize the alkali-containing compound to produce an alkali salt tat functions as a supplemental freezing point depressant; and applying the fluid onto a deicing solid to produce a coated deicing solid having reduced corrosiveness compared to the deicing solid not coated with the fluid. 35. A process according to claim 34 wherein the deicing solid is a road salt.
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