Strobe desorption method for high boiling point materials
원문보기
IPC분류정보
국가/구분
United States(US) Patent
등록
국제특허분류(IPC7판)
G01N-001/22
G01N-001/24
출원번호
US-0081006
(2005-03-14)
등록번호
US-7299679
(2007-11-27)
발명자
/ 주소
Lovell,John Stanley
French,Patrick D.
Barringer,Anthony Ren챕
출원인 / 주소
ADA Technologies, Inc.
대리인 / 주소
Sheridan Ross P.C.
인용정보
피인용 횟수 :
4인용 특허 :
34
초록▼
The invention is directed to a system and method for detecting substances, such as high boiling and low vapor pressure materials, using high energy radiation imparted by a suitable radiation source, such as a strobe or laser over a short time period. The radiation source causes the materials to vapo
The invention is directed to a system and method for detecting substances, such as high boiling and low vapor pressure materials, using high energy radiation imparted by a suitable radiation source, such as a strobe or laser over a short time period. The radiation source causes the materials to vaporize. A system handling system is used in conjunction with a detector to detect the presence of the materials including explosives, explosive-related compounds, chemical warfare agents, drugs, toxic industrial compounds, and derivatives thereof.
대표청구항▼
What is claimed is: 1. A method for detecting a high boiling point and/or a low vapor pressure material, comprising: providing a housing comprising an inlet, a strobe, a gas source, and a detector, wherein the housing at least substantially surrounds the strobe and the inlet and wherein the inlet i
What is claimed is: 1. A method for detecting a high boiling point and/or a low vapor pressure material, comprising: providing a housing comprising an inlet, a strobe, a gas source, and a detector, wherein the housing at least substantially surrounds the strobe and the inlet and wherein the inlet is positioned between the strobe and a surface potentially comprising a high boiling point and/or low vapor pressure material; directing radiation from the strobe onto the surface to volatilize the high boiling point and/or low vapor pressure material, the directing radiation step is conducted over a time period of no more than about 1/100th seconds; transporting an airborne sample comprising at least a portion of any volatilized high boiling point and/or low vapor pressure materials on the surface through the inlet and through a heated conduit to the detector, wherein an internal surface of the heated conduit is maintained at a temperature sufficient to inhibit absorption and/or condensation of the high boiling point and/or low vapor pressure material on the internal surface, and wherein the heated conduit extends from the inlet to the detector; and detecting whether or not the high boiling point and/or low vapor pressure material is present in the collected sample. 2. The method of claim 1, wherein said transporting further comprises directing a pressurized stream of gas from the gas source onto and/or around said surface at a flow rate sufficient to transport the gaseous stream and any high boiling point and/or low vapor pressure materials on the surface upward through the inlet of the housing and through the heated conduit after contact of the gaseous stream with the surface. 3. The method of claim 1, wherein said transporting step further comprises maintaining a negative pressure in the vicinity of the surface to draw said sample through the inlet of the housing and through the heated conduit. 4. The method of claim 1, wherein the temperature of the heated conduit ranges from about 100째 C. to about 250째 C., and wherein the temperature of the heated conduit is at least the condensation temperature of the material. 5. The method of claim 1, wherein the strobe comprises a xenon flash tube, and wherein said directing radiation step further comprises directing at least about 200 Joules of cumulative energy onto the surface. 6. The method of claim 1, wherein the high boiling point and/or low vapor pressure material is at least one of an explosive, an explosive related compound, a chemical warfare agent, a drug, a toxic industrial compound, and derivatives thereof, and wherein the radiation has one or more wavelengths in the range of from about 300 nm to about 700 nm in the visible region and/or from about 700 nm to about 2 microns in the infrared region of the electromagnetic spectrum. 7. The method of claim 1, wherein an offset distance between a surface of the strobe and the surface is no more than about 5 cm. 8. The method of claim 1, further comprising before the directing radiation step: applying a volatilizing agent to the surface, wherein the volatilizing agent is at least one of water, a volatile organic solvent, and mixtures thereof; wherein the strobe has an outputted energy profile, and wherein a peak of the profile is located in a radiation absorption band of the volatilizing agent. 9. The method of claim 1, wherein the strobe has an outputted energy profile, and wherein a peak of the profile is located in a radiation absorption band of the material. 10. A system for detecting a high boiling point and/or a low vapor pressure material, comprising: a strobe operable to direct radiation onto a surface potentially comprising a high boiling point and/or low vapor pressure material over a time period of no more than about 1/100th seconds to volatilize the high boiling point and/or low vapor pressure material; a housing at least substantially surrounding the strobe and an inlet to the housing, said housing comprising a sample handling system operable to collect an airborne sample comprising at least a portion of any volatilized high boiling point and/or low vapor pressure materials at and/or near the surface; and a detector operable to detect whether or not the high boiling point and/or low vapor pressure material is present in the collected sample; wherein said sample handling system comprises a heated conduit extending substantially from the inlet to the detector and a means for transporting said collected airborne sample through said heated conduit to said detector, wherein an internal surface of the heated conduit is maintained at a temperature sufficient to inhibit absorption and/or condensation of the high boiling point and/or low vapor pressure material on the internal surface. 11. The system of claim 10, further comprising a gas source for directing a stream of pressurized gas onto the surface at a flow rate sufficient to transport the gaseous stream and any high boiling point and/or low vapor pressure materials on said surface upward through the inlet of the housing and through the heated conduit after contact of the gaseous stream with the surface. 12. The system of claim 10, wherein the sample handling system further comprises a vacuum pump to maintain a negative pressure in the vicinity of the surface. 13. The system of claim 10, wherein the temperature of the heated conduit ranges from about 100째 C. to about 250째 C., and wherein the temperature of the heated conduit is at least the condensation temperature of the material. 14. The system of claim 10, wherein the strobe comprises a xenon flash tube wherein the high boiling point and/or low vapor pressure material is at least one of an explosive, an explosive related compound, a chemical warfare agent, a drug, a toxic industrial compound, and derivatives thereof, and wherein the radiation has one or more wavelengths in the range of from about 300 nm to about 700 nm in the visible region and/or from about 700 nm to about 2 microns in the infrared region of the electromagnetic spectrum. 15. The system of claim 10, further comprising an applicator operable to apply a volatilizing agent to the surface before radiation is contacted with the surface; wherein the strobe has an outputted energy profile, and wherein a peak of the profile is located in a radiation absorption band of the volatilizing agent. 16. A system for detecting a high boiling point and/or a low vapor pressure material, comprising: a strobe operable to direct radiation onto a surface potentially comprising a high boiling point and/or low vapor pressure material to volatilize the high boiling point and/or low vapor pressure material, wherein radiation emission cycles of the strobe are repeated at a frequency of at least about 0.2 Hz; a housing at least substantially surrounding the strobe and an inlet to the housing, said housing comprising a sample handling system operable to collect an airborne sample comprising at least a portion of any volatilized high boiling point and/or low vapor pressure materials at and/or near the surface; and a detector operable to detect whether or not the high boiling point and/or low vapor pressure material is present in the collected sample; wherein said sample handling system comprises a heated conduit extending substantially from the inlet to the detector and a means for transporting said collected airborne sample through said heated conduit to said detector, wherein an internal surface of the heated conduit is maintained at a temperature sufficient to inhibit absorption and/or condensation of the high boiling point and/or low vapor pressure material on the internal surface. 17. The system of claim 16, further comprising a gas source for directing a stream of pressurized gas onto the surface at a flow rate sufficient to transport the gaseous stream and any high boiling point and/or low vapor pressure materials on said surface upward through the inlet of the housing and through the heated conduit after contact of the gaseous stream with the surface. 18. The system of claim 16, wherein the sample handling system further comprises a vacuum pump to maintain a negative pressure in the vicinity of the surface. 19. The system of claim 16, wherein the temperature of the heated conduit ranges from about 100째 C. to about 250째 C., and wherein the temperature of the heated conduit is at least the condensation temperature of the material. 20. The system of claim 16, wherein the heated conduit comprises a glass and/or ceramic surface adjacent the transported sample, and wherein the heated conduit comprises a silanizing agent. 21. The method system of claim 16, wherein the heated conduit comprises an at least substantially nonpolar surface adjacent the transported sample. 22. The system of claim 16, wherein the strobe comprises a xenon flash tube wherein the high boiling point and/or low vapor pressure material is at least one of an explosive, an explosive related compound, a chemical warfare agent, a drug, a toxic industrial compound, and derivatives thereof, and wherein the radiation has one or more wavelengths in the range of from about 300 nm to about 700 nm in the visible region and/or from about 700 nm to about 2 microns in the infrared region of the electromagnetic spectrum.
연구과제 타임라인
LOADING...
LOADING...
LOADING...
LOADING...
LOADING...
이 특허에 인용된 특허 (34)
Parker ; III Frank M. (31535 Nichols Sawmill Rd. Magnolia TX 77355) Lucas David A. (300 Lazy La. Magnolia TX 77355), Apparatus and method for sampling hazardous material.
O\Brien Stephen E. (Bolton MA) Fine David H. (Sudbury MA) Fraim Freemand W. (Lexington MA), Detection method for checking surfaces for nitrogen-containing explosives or drugs.
Bleuse Patrick,FRX ; Clausin Pierre,FRX ; Heurtel Christian,FRX, Device for sampling gaseous substances, liquids, aerosols or even powdered materials for in situ analysis.
Fisher William H. (Thornhill CAX) Stott William R. (Aurora CAX) Thomson Bruce A. (Etobicoke CAX) Weisz-Margulescu Adam (Thornhill CAX), Method and apparatus for trace sample collection.
Aker, Craig A.; Cumming, Colin J.; Fisher, Mark E.; Fox, Michael J.; laGrone, Marcus J.; Reust, Dennis K.; Rockley, Mark G.; Towers, Eric S., Vapor sensing instrument for ultra trace chemical detection.
※ AI-Helper는 부적절한 답변을 할 수 있습니다.