Lithographic projection apparatus, purge gas supply system and gas purging method
원문보기
IPC분류정보
국가/구분
United States(US) Patent
등록
국제특허분류(IPC7판)
B01D-053/22
G03B-021/14
출원번호
UP-0565486
(2004-07-21)
등록번호
US-7789940
(2010-09-27)
국제출원번호
PCT/US2004/023490
(2004-07-21)
§371/§102 date
20060504
(20060504)
국제공개번호
WO05/010619
(2005-02-03)
발명자
/ 주소
Parekh, Bipin S.
Spiegelman, Jeffrey J.
Zeller, Robert S.
Holmes, Russell J.
출원인 / 주소
Entegris, Inc.
대리인 / 주소
Hamilton, Brook, Smith & Reynolds, P.C.
인용정보
피인용 횟수 :
0인용 특허 :
32
초록▼
A lithographic projection apparatus (1) includes a support configured to support a patterning device (MA), the patterning device configured to pattern the projection beam according to a desired pattern. The apparatus has a substrate (W) table configure to hold a substrate, a projection system config
A lithographic projection apparatus (1) includes a support configured to support a patterning device (MA), the patterning device configured to pattern the projection beam according to a desired pattern. The apparatus has a substrate (W) table configure to hold a substrate, a projection system configured to project the patterned beam onto a target portion of the substrate. The apparatus also has a purge gas supply system (100) configured to provide a purge gas near a surface of a component of the lithographic projection apparatus. The purge gas supply system (100) includes a purge gas mixture generator (120) configured to generate a purge gas mixture which includes at least one purging gas and moisture. The purge gas mixture generator has a moisturizer (150) configured to add the moisture to the purge gas and a purge gas mixture outlet (130) connected to the purge gas mixture generator (120) configured to supply the purge gas mixture near the surface.
대표청구항▼
What is claimed is: 1. A purge gas mixture supply system, comprising: a purge gas mixture generator comprising a moisturizer configured to add moisture to a purge gas, wherein said moisturizer comprises a first region containing a purge gas flow and a second region containing water wherein the firs
What is claimed is: 1. A purge gas mixture supply system, comprising: a purge gas mixture generator comprising a moisturizer configured to add moisture to a purge gas, wherein said moisturizer comprises a first region containing a purge gas flow and a second region containing water wherein the first and second regions are separated by a membrane contactor that forms a hollow fiber that is gas permeable and substantially resistant to liquid intrusion, one of the first and second regions being within the fiber and the other of the first and second regions being outside the fiber; the purge gas mixture generator being configured to add the moisture to the purge gas by further comprising a mass flow controller to control flow rate of the purge gas flow through the first region of the moisturizer and a pressure regulator to control flow of the water through the second region of the moisturizer such that the moisture is added to the purge gas to create a humidified purge gas mixture; and a purge gas mixture outlet being connected to the purge gas mixture generator to supply the humidified purge gas mixture to at least part of a lithographic projection apparatus. 2. The supply system of claim 1, wherein the membrane contactor is comprised of a thermoplastic polymer. 3. The supply system of claim 1, wherein the membrane contactor is comprised of a perfluorinated polymer. 4. The supply system of claim 3, wherein the perfluorinated polymer is polytetrafluoroethylene. 5. The supply system of claim 1, wherein the moisturizer comprises: a) a bundle of a plurality of gas-permeable hollow fiber membranes having a first end and a second end, said membranes having an outer surface and an inner surface, said inner surface comprising one of the first and second regions; b) each end of said bundle potted with a liquid tight seal forming an end structure with a surrounding housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines the other of the first and second regions between the inner wall and the hollow fiber membranes; d) said housing comprising a purge gas inlet connected to a purge gas source, and comprising the purge gas mixture outlet; and e) said housing comprising a water inlet connected to a water source, and comprising a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas mixture outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle, and wherein said purge gas mixture comprises at least one purge gas and the moisture. 6. A purge gas mixture supply system, comprising: a purge gas mixture generator comprising a moisturizer configured to add moisture to a purge gas, wherein said moisturizer comprises: a) a bundle of a plurality of perfluorinated gas-permeable thermoplastic hollow fiber membranes having a first end and a second end and being substantially resistant to liquid intrusion, said membranes having an outer surface and an inner surface, said inner surface comprising a lumen; b) each end of said bundle potted with a liquid tight perfluorinated thermoplastic seal forming a unitary end structure with a surrounding perfluorinated thermoplastic housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines a fluid flow volume between the inner wall and the hollow fiber membranes; d) said housing comprising a purge gas inlet connected to a purge gas source, and comprising a purge gas mixture outlet; and e) said housing comprising a water inlet connected to a water source, and comprising a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas mixture outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle, and wherein said purge gas mixture comprises at least one purge gas and the moisture; the purge gas mixture generator being configured to add the moisture to the purge gas by further comprising a mass flow controller to control flow rate of the purge gas flow through the moisturizer and a pressure regulator to control flow of the water through the moisturizer such that the moisture is added to the purge gas to create a humidified purge gas mixture; and the purge gas mixture outlet being connected to the purge gas mixture generator to supply the humidified purge gas mixture to at least part of a lithographic projection apparatus. 7. The supply system of claim 6, further comprising a heating device for the water. 8. The supply system of claim 6, wherein the purge gas source comprises a purifier device. 9. The supply system of claim 8, wherein the purifier device is regenerable. 10. The supply system of claim 9, wherein the purge gas source comprises two purifier devices and wherein the purifier devices are connected in parallel. 11. The supply system of claim 6, wherein the hollow fiber membranes are selected from the group consisting of: a) hollow fiber membranes having a porous skinned inner surface, a porous outer surface and a porous support structure between; b) hollow fiber membranes having a non-porous skinned inner surface, a porous outer surface and a porous support structure between; c) hollow fiber membranes having a porous skinned outer surface, a porous inner surface and a porous support structure between; and d) hollow fiber membranes having a non-porous skinned outer surface, a porous inner surface and a porous support structure between. 12. The supply system of claim 11, wherein the hollow fiber membrane outer diameter is about 350 microns to about 1450 microns. 13. The supply system of claim 12, wherein the hollow fiber membranes are hollow fiber membranes having a porous skinned inner surface, a porous outer surface and a porous support structure between; or hollow fiber membranes having a porous skinned outer surface, a porous inner surface and a porous support structure between; and the porous skinned surface pores are from about 0.001 microns to about 0.005 microns in diameter. 14. The supply system of claim 6, wherein the first and second ends of the bundle are potted with a liquid tight perfluorinated thermoplastic seal forming a single unitary end structure comprising both the first and second ends with a surrounding perfluorinated thermoplastic housing wherein the fibers of the ends are separately open to fluid flow. 15. The supply system of claim 6, wherein said supply system is capable of operation at a purge gas flow rate of at least about 30 standard liters per minute and a temperature of at least about 90° C. 16. The supply system of claim 6, wherein the purge gas mixture generator is heated for a sufficient length of time at a temperature sufficient to substantially remove compounds that volatilize at temperatures of about 100° C. or less. 17. A method of humidifying a purge gas, comprising: passing the purge gas through a moisturizer for a period sufficient to humidify the purge gas, wherein the moisturizer comprises a first region containing a purge gas flow and a second region containing water wherein the first and second regions are separated by a gas-permeable membrane that forms a hollow fiber and is substantially resistant to liquid intrusion, one of the first and second regions being within the fiber and the other of the first and second regions being outside the fiber; controlling flow rate of the purge gas flow through the first region of the moisturizer with a mass flow controller and controlling flow of the water through the second region of the moisturizer with a pressure regulator such that moisture is added to the purge gas to create a humidified purge gas mixture; and supplying the humidified purge gas mixture to at least part of a lithographic projection apparatus. 18. A method of humidifying a purge gas, comprising passing the purge gas through a moisturizer for a period sufficient to humidify the purge gas, wherein the moisturizer comprises: a) a bundle of a plurality of perfluorinated gas-permeable thermoplastic hollow fiber membranes having a first end and a second end and being substantially resistant to liquid intrusion, said membranes having an outer surface and an inner surface, said inner surface comprising a lumen; b) each end of said bundle potted with a liquid tight perfluorinated thermoplastic seal forming a unitary end structure with a surrounding perfluorinated thermoplastic housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines a fluid flow volume between the inner wall and the hollow fiber membranes; d) said housing comprising a purge gas inlet connected to a purge gas source, and comprising a purge gas outlet; and e) said housing having a water inlet connected to a water source and a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle, thereby obtaining a humidified purge gas; the method further comprising controlling flow rate of the purge gas flow through the moisturizer with a mass flow controller and controlling flow of the water through the moisturizer with a pressure regulator such that moisture is added to the purge gas; and supplying the humidified purge gas through the purge gas outlet to at least part of a lithographic projection apparatus. 19. A lithographic projection apparatus, comprising: an illuminator configured to provide a projection beam of radiation; a support structure configured to support a patterning device, the patterning device configured to pattern the projection beam according to a desired pattern; a substrate table configured to hold a substrate; a projection system configured to project the patterned beam onto a target portion of the substrate; and at least one purge gas supply system configured to provide a purge gas to at least part of the lithographic projection apparatus, the at least one purge gas supply system comprising: a purge gas mixture generator comprising a moisturizer configured to add moisture to a purge gas, wherein the moisturizer comprises a first region containing a purge gas flow and a second region containing water wherein the first and second regions are separated by a gas-permeable membrane that forms a hollow fiber and is substantially resistant to liquid intrusion, one of the first and second regions being within the fiber and the other of the first and second regions being outside the fiber, the purge gas mixture generator configured to generate a purge gas mixture, which purge gas mixture comprises at least one purge gas and the moisture, the purge gas mixture generator being configured to add the moisture to the purge gas by further comprising a mass flow controller to control flow rate of the purge gas flow through the first region of the moisturizer and a pressure regulator to control flow of the water through the second region of the moisturizer such that the moisture is added to the purge gas; and a purge gas mixture outlet connected to the purge gas mixture generator configured to supply the purge gas mixture to the at least part of the lithographic projection apparatus. 20. A lithographic projection apparatus, comprising: an illuminator configured to provide a projection beam of radiation; a support structure configured to support a patterning device, the patterning device configured to pattern the projection beam according to a desired pattern; a substrate table configured to hold a substrate; a projection system configured to project the patterned beam onto a target portion of the substrate; and at least one purge gas supply system configured to provide a purge gas to at least part of the lithographic projection apparatus, the at least one purge gas supply system comprising: a purge gas mixture generator comprising a moisturizer configured to add moisture to a purge gas, wherein the moisturizer comprises: a) a bundle of a plurality of perfluorinated gas-permeable thermoplastic hollow fiber membranes having a first end and a second end and being substantially resistant to liquid intrusion, said membranes having an outer surface and an inner surface, said inner surface comprising a lumen; b) each end of said bundle potted with a liquid tight perfluorinated thermoplastic seal forming a unitary end structure with a surrounding perfluorinated thermoplastic housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines a fluid flow volume between the inner wall and the hollow fiber membranes; d) said housing comprising a purge gas inlet connected to a purge gas source, and comprising a purge gas mixture outlet; and e) said housing comprising a water inlet connected to a water source, and comprising a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas mixture outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle, the purge gas mixture generator configured to generate a purge gas mixture, which purge gas mixture comprises at least one purge gas and the moisture, the purge gas mixture generator being configured to add the moisture to the purge gas by further comprising a mass flow controller to control flow rate of the purge gas flow through the moisturizer and a pressure regulator to control flow of the water through the moisturizer such that the moisture is added to the purge gas; and a purge gas mixture outlet connected to the purge gas mixture generator configured to supply the purge gas mixture to the at least part of the lithographic projection apparatus. 21. A method for providing a purge gas to at least part of a lithographic projection apparatus comprising: an illuminator configured to provide a projection beam of radiation; a support configured to support a patterning device, the patterning device configured to pattern the projection beam according to a desired pattern; a substrate table configured to hold a substrate; and a projection system configured to project the patterned beam onto a target portion of the substrate; the method comprising: generating a purge gas mixture which comprises at least one purge gas and moisture by adding moisture to a purge gas with a moisturizer, wherein the moisturizer comprises a first region containing a purge gas flow and a second region containing water wherein the first and second regions are separated by a gas-permeable membrane that forms a hollow fiber and is substantially resistant to liquid intrusion, one of the first and second regions being within the fiber and the other of the first and second regions being outside the fiber; and supplying the purge gas mixture to at least a part of the lithographic projection apparatus; the method further comprising controlling flow rate of the purge gas flow through the first region of the moisturizer with a mass flow controller and controlling flow of the water through the second region of the moisturizer with a pressure regulator such that the moisture is added to the purge gas. 22. A method for providing a purge gas to at least part of a lithographic projection apparatus comprising: an illuminator configured to provide a projection beam of radiation; a support configured to support a patterning device, the patterning device configured to pattern the projection beam according to a desired pattern; a substrate table configured to hold a substrate; and a projection system configured to project the patterned beam onto a target portion of the substrate; the method comprising: generating a purge gas mixture which comprises at least one purge gas and moisture by adding moisture to a purge gas with a moisturizer, wherein the moisturizer comprises: a) a bundle of a plurality of perfluorinated gas-permeable thermoplastic hollow fiber membranes having a first end and a second end and being substantially resistant to liquid intrusion, said membranes having an outer surface and an inner surface, said inner surface comprising a lumen; b) each end of said bundle potted with a liquid tight perfluorinated thermoplastic seal forming a unitary end structure with a surrounding perfluorinated thermoplastic housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines a fluid flow volume between the inner wall and the hollow fiber membranes; d) said housing having a purge gas inlet connected to a purge gas source and a purge gas mixture outlet; and e) said housing having a water inlet connected to a water source and a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas mixture outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle, and supplying the purge gas mixture to at least a part of the lithographic projection apparatus; the method further comprising controlling flow rate of the purge gas flow through the moisturizer with a mass flow controller and controlling flow of the water through the moisturizer with a pressure regulator such that the moisture is added to the purge gas. 23. The lithographic projection apparatus of claim 19, wherein the membrane is comprised of a thermoplastic polymer. 24. The lithographic projection apparatus of claim 19, wherein the membrane is comprised of a perfluorinated polymer. 25. The lithographic projection apparatus of claim 24, wherein the perfluorinated polymer is polytetrafluoroethylene. 26. The lithographic projection apparatus of claim 19, wherein the moisturizer comprises: a) a bundle of a plurality of gas-permeable hollow fiber membranes having a first end and a second end, said membranes having an outer surface and an inner surface, said inner surface comprising one of the first and second regions; b) each end of said bundle potted with a liquid tight seal forming an end structure with a surrounding housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines the other of the first and second regions between the inner wall and the hollow fiber membranes; d) said housing comprising a purge gas inlet connected to a purge gas source, and comprising a purge gas mixture outlet; and e) said housing comprising a water inlet connected to a water source, and comprising a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas mixture outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle. 27. The lithographic projection apparatus of claim 20, further comprising a heating device for the water. 28. The lithographic projection apparatus of claim 20, wherein the purge gas source comprises a purifier device. 29. The lithographic projection apparatus of claim 28, wherein the purifier device is regenerable. 30. The lithographic projection apparatus of claim 29, wherein the purge gas source comprises two purifier devices and wherein the purifier devices are connected in parallel. 31. The lithographic projection apparatus of claim 20, wherein the hollow fiber membranes are selected from the group consisting of: a) hollow fiber membranes having a porous skinned inner surface, a porous outer surface and a porous support structure between; b) hollow fiber membranes having a non-porous skinned inner surface, a porous outer surface and a porous support structure between; c) hollow fiber membranes having a porous skinned outer surface, a porous inner surface and a porous support structure between; and d) hollow fiber membranes having a non-porous skinned outer surface, a porous inner surface and a porous support structure between. 32. The lithographic projection apparatus of claim 31, wherein the hollow fiber membrane outer diameter is about 350 microns to about 1450 microns. 33. The lithographic projection apparatus of claim 31, wherein the hollow fiber membranes are hollow fiber membranes having a porous skinned inner surface, a porous outer surface and a porous support structure between; or hollow fiber membranes having a porous skinned outer surface, a porous inner surface and a porous support structure between; and the porous skinned surface pores are from about 0.001 microns to about 0.005 microns in diameter. 34. The lithographic projection apparatus of claim 20, wherein the first and second ends of the bundle are potted with a liquid tight perfluorinated thermoplastic seal forming a single unitary end structure comprising both the first and second ends with a surrounding perfluorinated thermoplastic housing wherein the fibers of the ends are separately open to fluid flow. 35. The lithographic projection apparatus of claim 20, wherein said supply system is capable of operation at a purge gas flow rate of at least about 30 standard liters per minute and a temperature of at least about 90° C. 36. The lithographic projection apparatus of claim 20, wherein the purge gas mixture generator is heated for a sufficient length of time at a temperature sufficient to substantially remove compounds that volatilize at temperatures of about 100° C. or less. 37. The method of claim 17, wherein the membrane is comprised of a thermoplastic polymer. 38. The method of claim 17, wherein the membrane is comprised of a perfluorinated polymer. 39. The method of claim 38, wherein the perfluorinated polymer is polytetrafluoroethylene. 40. The method of claim 17, wherein the moisturizer comprises: a) a bundle of a plurality of gas-permeable hollow fiber membranes having a first end and a second end, said membranes having an outer surface and an inner surface, said inner surface comprising one of the first and second regions; b) each end of said bundle potted with a liquid tight seal forming an end structure with a surrounding housing wherein the fiber ends are open to fluid flow; c) said housing having an inner wall and an outer wall, wherein the inner wall defines the other of the first and second regions between the inner wall and the hollow fiber membranes; d) said housing comprising a purge gas inlet connected to a purge gas source, and comprising a purge gas mixture outlet; and e) said housing comprising a water inlet connected to a water source, and comprising a water outlet, wherein either the purge gas inlet is connected to the first end of the bundle and the purge gas mixture outlet is connected to the second end of the bundle or the water inlet is connected to the first end of the bundle and the water outlet is connected to the second end of the bundle. 41. The method of claim 18, wherein the water is heated in or prior to entering the moisturizer. 42. The method of claim 18, wherein the purge gas source comprises a purifier device. 43. The method of claim 42, wherein the purifier device is regenerable. 44. The method of claim 43, wherein the purge gas source comprises first and second purifier devices and wherein the purifier devices are connected in parallel. 45. The method of claim 44, wherein the purge gas is purified by either the first or the second purifier device and wherein the other purifier device is regenerated. 46. The method of claim 18, wherein the hollow fiber membranes are selected from the group consisting of: a) hollow fiber membranes having a porous skinned inner surface, a porous outer surface and a porous support structure between; b) hollow fiber membranes having a non-porous skinned inner surface, a porous outer surface and a porous support structure between; c) hollow fiber membranes having a porous skinned outer surface, a porous inner surface and a porous support structure between; and d) hollow fiber membranes having a non-porous skinned outer surface, a porous inner surface and a porous support structure between. 47. The method of claim 46, wherein the hollow fiber membrane outer diameter is about 350 microns to about 1450 microns. 48. The method of claim 46, wherein the hollow fiber membranes are hollow fiber membranes having a porous skinned inner surface, a porous outer surface and a porous support structure between or hollow fiber membranes having a porous skinned outer surface, a porous inner surface and a porous support structure between and the porous skinned surface pores are from about 0.001 microns to about 0.005 microns in diameter. 49. The method of claim 18, wherein the first and second ends of the bundle are potted with a liquid tight perfluorinated thermoplastic seal forming a single unitary end structure comprising both the first and second ends with a surrounding perfluorinated thermoplastic housing wherein the fibers of the ends are separately open to fluid flow. 50. The method of claim 18, wherein the temperature of the water is at least about 30° C. 51. The method of claim 50, wherein the temperature of the water is at least about 50° C. 52. The method of claim 18, wherein the flow rate of the purge gas is at least about 20 standard liters per minute. 53. The method of claim 52, wherein the flow rate of the purge gas is at least about 60 standard liters per minute. 54. The method of claim 18, wherein the relative humidity of the humidified purge gas is at least about 20%. 55. The method of claim 54, wherein the relative humidity of the humidified purge gas is at least about 50%. 56. The method of claim 55, wherein the humidified purge gas is substantially saturated with moisture. 57. The method of claim 18, wherein the purge gas entering the moisturizer comprises no greater than about 1 part per billion (ppb) contaminants and wherein the humidified purge gas leaving the moisturizer comprises no greater than about 1 ppb contaminants. 58. The method of claim 57, wherein the purge gas entering the moisturizer comprises no greater than about 100 parts per trillion (ppt) contaminants and wherein the humidified purge gas leaving the moisturizer comprises no greater than about 100 ppt contaminants. 59. The method of claim 58, wherein the purge gas entering the moisturizer comprises no greater than about 1 ppt contaminants and wherein the humidified purge gas leaving the moisturizer comprises no greater than about 1 ppt contaminants. 60. A purge gas mixture supply system, comprising: a purge gas mixture generator comprising a moisturizer configured to add moisture to a purge gas, wherein said moisturizer comprises a first region containing a purge gas flow and a second region containing water wherein the first and second regions are separated by a membrane contactor; the purge gas mixture generator being configured to add the moisture to the purge gas by further comprising a mass flow controller to control flow rate of the purge gas flow through the first region of the moisturizer and a pressure regulator to control flow of the water through the second region of the moisturizer such that the moisture is added to the purge gas to create a humidified purge gas mixture; and a purge gas mixture outlet being connected to the purge gas mixture generator to supply the humidified purge gas mixture to at least part of a lithographic projection apparatus. 61. The supply system of claim 60, wherein the membrane contactor comprises a perfluorosulfonic acid polytetrafluoroethylene copolymer membrane. 62. The supply system of claim 60, wherein the membrane contactor comprises a membrane comprising a substance suitable for use as a fuel cell humidifier. 63. The supply system of claim 60, wherein the membrane contactor comprises an ionomer. 64. The supply system of claim 62, wherein the membrane contactor comprises a sulfonated tetrafluoroethylene based fluoropolymer-copolymer membrane. 65. The supply system of claim 64, wherein the membrane contactor comprises a perfluorosulfonic acid polytetrafluoroethylene copolymer membrane. 66. The supply system of claim 60, further comprising a heating device for the water. 67. The supply system of claim 60, further comprising a purifier device for a purge gas source. 68. The supply system of claim 67, wherein the purifier device is regenerable. 69. The supply system of claim 68, wherein the purge gas source comprises two purifier devices and wherein the purifier devices are connected in parallel. 70. The supply system of claim 60, wherein said supply system is capable of operation at a purge gas flow rate of at least about 30 standard liters per minute and a temperature of at least about 90° C. 71. The supply system of claim 60, wherein the purge gas mixture generator is heated for a sufficient length of time at a temperature sufficient to substantially remove compounds that volatilize at temperatures of about 100° C. or less. 72. The supply system of claim 60, wherein the relative humidity of the humidified purge gas is at least about 50%. 73. The supply system of claim 60, wherein the purge gas entering the moisturizer comprises no greater than about 1 part per billion (ppb) contaminants and wherein the humidified purge gas leaving the moisturizer comprises no greater than about 1 ppb contaminants.
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