[논문]High-performance porous carbon-zeolite mixed-matrix membranes for CO2/N2 separation

Chuah, Chong Yang; Lee, Junghyun; Bao, Yueping; Song, Juha; Bae, Tae-Hyun

doi:10.1016/j.memsci.2020.119031

[해외논문] High-performance porous carbon-zeolite mixed-matrix membranes for CO2/N2 separation

Journal of membrane science, v.622, 2021년, pp.119031 -

Chuah, Chong Yang (Singapore Membrane Technology Centre, Nanyang Environment and Water Research Institute) , Lee, Junghyun (School of Chemical and Biomedical Engineering, Nanyang Technological University) , Bao, Yueping (Environmental Chemistry and Materials Centre, Nanyang Environment and Water Research Institute) , Song, Juha (School of Chemical and Biomedical Engineering, Nanyang Technological University) , Bae, Tae-Hyun (Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology)

Abstract ▼ AI-Helper

Abstract Nano-sized PS-MFI, ETS-10 and SAPO-34 zeolites were utilized as CO2-selective fillers to fabricate high-performance mixed-matrix carbon molecular sieve membranes (CMSMs) for application in the CO2/N2 separation process. In this work, an in-house polyimide, ODPA-TMPDA, was used as a polymer precursor for CMSMs, due to its higher intrinsic gas permeability compared with commercial polyimides. Zeolite-filled CMSMs were then successfully fabricated without any appreciable defects at the filler/matrix interfaces. Gas permeation testing revealed that both CO2 permeability and CO2/N2 selectivity can be significantly improved upon incorporation of such zeolite fillers, enabling selective adsorption and transport of CO2. In particular, SAPO-34 yielded the best results among the zeolite fillers tested, resulting in an excellent performance far beyond the Robeson upper bound limit for CO2/N2 separation. Highlights PS-MFI, ETS-10 and SAPO-34 nanoparticles were synthesized. ODPA-TMPDA polyimide was used as a precursor for the porous carbon matrix. Various zeolite nanoparticles were incorporated in the porous carbon matrix. Mixed-matrix carbon molecular sieve membranes showed outstanding CO2/N2 separation performance. Graphical abstract [DISPLAY OMISSION]

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