[논문]Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying

Huang, Chih-Chieh; Lam, Tu-Ngoc; Amalia, Lia; Chen, Kuan-Hung; Yang, Kuo-Yi; Muslih, M. Rifai; Singh, Sudhanshu Shekhar; Tsai, Pei-I.; Lee, Yuan-Tzu; Jain, Jayant; Lee, Soo Yeol; Lai, Hong-Jen; Huang, Wei-Chin; Chen, San-Yuan; Huang, E-Wen

doi:10.1038/s41598-021-89022-9

[해외논문] Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying 원문보기

Scientific reports, v.11 no.1, 2021년, pp.9610 -

Huang, Chih-Chieh (Department of Materials Science and Engineering, National Yang Ming Chiao Tung University, Hsinchu, 30013 Taiwan) , Lam, Tu-Ngoc (Department of Materials Science and Engineering, National Yang Ming Chiao Tung University, Hsinchu, 30013 Taiwan) , Amalia, Lia (Department of Materials Science and Engineering, National Yang Ming Chiao Tung University, Hsinchu, 30013 Taiwan) , Chen, Kuan-Hung (Department of Materials Science and Engineering, National Yang Ming Chiao Tung University, Hsinchu, 30013 Taiwan) , Yang, Kuo-Yi (Biomedical Technology and Device Research Laboratories, Industrial Technology Research Institute, Hsinchu, 310 Taiwan) , Muslih, M. Rifai (Neutron Scattering Lab. PSTBM-BATAN, Kawasan PUSPIPTEK Serpong, 15314 Indonesia) , Singh, Sudhanshu Shekhar (Department of Materials Science and Engineering, Indian Institute of Technology Kanpur, Kanpur, UP 208016 India) , Tsai, Pei-I. (Biomedical Technology and Device Research Laboratories, Industrial Technology Research Institute, Hsinchu, 310 Taiwan) , Lee, Yuan-Tzu (Department of Materials Science and Engineering, National Taiwan University, Taipei, 10607 Taiwan) , Jain, Jayant (Depa) , Lee, Soo Yeol , Lai, Hong-Jen , Huang, Wei-Chin , Chen, San-Yuan , Huang, E-Wen

Abstract ▼ AI-Helper

We demonstrated the design of pre-additive manufacturing microalloying elements in tuning the microstructure of iron (Fe)-based alloys for their tunable mechanical properties. We tailored the microalloying stoichiometry of the feedstock to control the grain sizes of the metallic alloy systems. Two specific microalloying stoichiometries were reported, namely biodegradable iron powder with 99.5% purity (BDFe) and that with 98.5% (BDFe-Mo). Compared with the BDFe, the BDFe-Mo powder was found to have lower coefficient of thermal expansion (CTE) value and better oxidation resistance during consecutive heating and cooling cycles. The selective laser melting (SLM)-built BDFe-Mo exhibited high ultimate tensile strength (UTS) of 1200 MPa and fair elongation of 13.5%, while the SLM-built BDFe alloy revealed a much lower UTS of 495 MPa and a relatively better elongation of 17.5%, indicating the strength enhancement compared with the other biodegradable systems. Such an enhanced mechanical behavior in the BDFe-Mo was assigned to the dominant mechanism of ferrite grain refinement coupled with precipitate strengthening. Our findings suggest the tunability of outstanding strength-ductility combination by tailoring the pre-additive manufacturing microalloying elements with their proper concentrations.

참고문헌 (79)

1. Costello, K. & Rimol M. Gartner Identifies Five Emerging Trends That Will Drive Technology Innovation for the Next Decade . 2020: STAMFORD, Conn. p. https://www.gartner.com/en/newsroom/press-releases/2020-08-18-gartner-identifies-five-emerging-trends-that-will-drive-technology-innovation-for-the-next-decade .
2. Middleton JC Tipton AJ Synthetic biodegradable polymers as orthopedic devices Biomaterials 2000 21 23 2335 2346 10.1016/S0142-9612(00)00101-0 11055281

상세보기
3. Gilding DK Reed AM Biodegradable polymers for use in surgery―polyglycolic/poly(actic acid) homo- and copolymers: 1 Polymer 1979 20 12 1459 1464 10.1016/0032-3861(79)90009-0

상세보기
4. Cha P-R Biodegradability engineering of biodegradable Mg alloys: Tailoring the electrochemical properties and microstructure of constituent phases Sci. Rep. 2013 3 1 2367 10.1038/srep02367 23917705

상세보기
5. Yang H Alloying design of biodegradable zinc as promising bone implants for load-bearing applications Nat. Commun. 2020 11 1 401 10.1038/s41467-019-14153-7 31964879

상세보기
6. Kannan MB Biocompatibility and biodegradation studies of a commercial zinc alloy for temporary mini-implant applications Sci. Rep. 2017 7 1 15605 10.1038/s41598-017-15873-w 29142320

상세보기
7. Yusop AHM Controlling the degradation kinetics of porous iron by poly(lactic-co-glycolic acid) infiltration for use as temporary medical implants Sci. Rep. 2015 5 1 11194 10.1038/srep11194 26057073

상세보기
8. Huang T Zheng Y Uniform and accelerated degradation of pure iron patterned by Pt disc arrays Sci. Rep. 2016 6 1 23627 10.1038/srep23627 27033380

상세보기
9. Witte F Biodegradable magnesium scaffolds: part 1: appropriate inflammatory response J. Biomed. Mater. Res. Part A 2007 81 3 748 756 10.1002/jbm.a.31170

상세보기
10. Sezer N Review of magnesium-based biomaterials and their applications J. Magn. Alloys 2018 6 1 23 43 10.1016/j.jma.2018.02.003

상세보기
11. Peuster M Long-term biocompatibility of a corrodible peripheral iron stent in the porcine descending aorta Biomaterials 2006 27 28 4955 4962 10.1016/j.biomaterials.2006.05.029 16765434

상세보기
12. Wegener B Development of a novel biodegradable porous iron-based implant for bone replacement Sci. Rep. 2020 10 1 9141 10.1038/s41598-020-66289-y 32499489

상세보기
13. Colombo A Karvouni E Biodegradable stents : "fulfilling the mission and stepping away" Circulation 2000 102 4 371 373 10.1161/01.CIR.102.4.371 10908206

상세보기
14. Chandra G Pandey A Biodegradable bone implants in orthopedic applications: a review Biocybern. Biomed. Eng. 2020 40 2 596 610 10.1016/j.bbe.2020.02.003

상세보기
15. Peuster M A novel approach to temporary stenting: degradable cardiovascular stents produced from corrodible metal―results 6？18 months after implantation into New Zealand white rabbits Heart 2001 86 5 563 10.1136/heart.86.5.563 11602554

상세보기
16. Carluccio D Challenges and opportunities in the selective laser melting of biodegradable metals for load-bearing bone scaffold applications Metall. Mater. Trans. A 2020 51 7 3311 3334 10.1007/s11661-020-05796-z

상세보기
17. Obayi CS Effect of grain sizes on mechanical properties and biodegradation behavior of pure iron for cardiovascular stent application Biomatter 2016 6 1 e959874 10.4161/21592527.2014.959874 25482336

상세보기
18. Huang EW Hardening steels by the generation of transient phase using additive manufacturing Intermetallics 2019 109 60 67 10.1016/j.intermet.2019.03.004

상세보기
19. Tseng JC Deformations of Ti-6Al-4V additive-manufacturing-induced isotropic and anisotropic columnar structures: insitu measurements and underlying mechanisms Addit. Manuf. 2020 35 101322 32835025
20. Chae H Unravelling thermal history during additive manufacturing of martensitic stainless steel J. Alloys Compd. 2021 857 157555 10.1016/j.jallcom.2020.157555 33071463

상세보기
21. Tsai P-I Multi-scale mapping for collagen-regulated mineralization in bone remodeling of additive manufacturing porous implants Mater. Chem. Phys. 2019 230 83 92 10.1016/j.matchemphys.2019.03.047

상세보기
22. Manakari V Parande G Gupta M Selective laser melting of magnesium and magnesium alloy powders: a review Metals 2017 7 1 2 10.3390/met7010002

상세보기
23. Zhang LC Review on manufacture by selective laser melting and properties of titanium based materials for biomedical applications Mater. Technol. 2016 31 2 66 76 10.1179/1753555715Y.0000000076
24. Song B Microstructure and tensile properties of iron parts fabricated by selective laser melting Opt. Laser Technol. 2014 56 451 460 10.1016/j.optlastec.2013.09.017

상세보기
25. Carluccio D Comparative study of pure iron manufactured by selective laser melting, laser metal deposition, and casting processes Adv. Eng. Mater. 2019 21 7 1900049 10.1002/adem.201900049

상세보기
26. Calcagnotto M Orientation gradients and geometrically necessary dislocations in ultrafine grained dual-phase steels studied by 2D and 3D EBSD Mater. Sci. Eng. Struct. Mater. Prop. Microstruct. Process. 2010 527 10？11 2738 2746 10.1016/j.msea.2010.01.004

상세보기
27. Peng-Heng C Preban AG The effect of ferrite grain size and martensite volume fraction on the tensile properties of dual phase steel Acta Metall. 1985 33 5 897 903 10.1016/0001-6160(85)90114-2

상세보기
28. Jiang Z Guan Z Lian J Effects of microstructural variables on the deformation behaviour of dual-phase steel Mater. Sci. Eng. A 1995 190 1 55 64 10.1016/0921-5093(94)09594-M

상세보기
29. Lenka S Effect of recalescence on microstructure and phase transformation in high carbon steel Mater. Sci. Technol. 2013 29 6 715 725 10.1179/1743284713Y.0000000205

상세보기
30. Yokota T Mateo CG Bhadeshia HKDH Formation of nanostructured steels by phase transformation Scr. Mater. 2004 51 8 767 770 10.1016/j.scriptamat.2004.06.006

상세보기
31. Bajaj P Steels in additive manufacturing: a review of their microstructure and properties Mater. Sci. Eng. A 2020 772 138633 10.1016/j.msea.2019.138633

상세보기
32. Sigel A Sigel H Sigel RKO Interrelations between essential metal ions and human diseases Metal Ions Life Sci. 2013 13 415 450 10.1007/978-94-007-7500-8_13

상세보기
33. Redlich C Quadbeck P Thieme M Kiebackb B Molybdenum―a biodegradable implant material for structural applications? Acta Biomater. 2020 104 241 251 10.1016/j.actbio.2019.12.031 31926333

상세보기
34. Tan JH Wong WLE Dalgarno KW An overview of powder granulometry on feedstock and part performance in the selective laser melting process Addit. Manuf. 2017 18 228 255
35. Abd-Elghany K Bourell DL Property evaluation of 304L stainless steel fabricated by selective laser melting Rapid Prototyp. J. 2012 18 5 420 428 10.1108/13552541211250418

상세보기
36. Touloukian YS Thermophysical Properties Research, Thermal Expansion: Metallic Elements and Alloys 1994 University Microfilms International
37. Hull F Effect of composition on thermal expansion of alloys used in power generation J. Mater. Eng. 1987 9 1 81 92 10.1007/BF02833790

상세보기
38. Aslam I Thermodynamic and kinetic behavior of low-alloy steels: an atomic level study using an Fe？Mn？Si？C modified embedded atom method (MEAM) potential Materialia 2019 8 100473 10.1016/j.mtla.2019.100473

상세보기
39. Gray D. E. American Institute of Physics Handbook, (1972).
40. Hudok D Properties and selection: irons, steels, and high-performance alloys Met. Handbook 1990 1 200 211
41. Kozlovskii YM Stankus SV The linear thermal expansion coefficient of iron in the temperature range of 130？1180 K J. Phys. Conf. Ser. 2019 1382 012181 10.1088/1742-6596/1382/1/012181

상세보기
42. Liu YC Sommer F Mittemeijer EJ Calibration of the differential dilatometric measurement signal upon heating and cooling; thermal expansion of pure iron Thermochim. Acta 2004 413 1 215 225 10.1016/j.tca.2003.10.005

상세보기
43. Denand B Carbon content evolution in austenite during austenitization studied by in situ synchrotron X-ray diffraction of a hypoeutectoid steel Materialia 2020 10 100664 10.1016/j.mtla.2020.100664

상세보기
44. Armentani E Esposito R Sepe R The effect of thermal properties and weld efficiency on residual stresses in welding J. Achiev. Mater. Manuf. Eng. 2007 1 146
45. Li C Residual stress in metal additive manufacturing Procedia CIRP 2018 71 348 353 10.1016/j.procir.2018.05.039

상세보기
46. Mercelis P Kruth JP Residual stresses in selective laser sintering and selective laser melting Rapid Prototyp. J. 2006 12 5 254 265 10.1108/13552540610707013

상세보기
47. Yakout M Elbestawi MA Veldhuis SC A study of thermal expansion coefficients and microstructure during selective laser melting of Invar 36 and stainless steel 316L Addit. Manuf. 2018 24 405 418
48. Liu S Oxide scales characterization of micro-alloyed steel at high temperature J. Mater. Process. Technol. 2013 213 7 1068 1075 10.1016/j.jmatprotec.2013.01.022

상세보기
49. Chen RY Yuen WYD Short-time oxidation behavior of low-carbon, low-silicon steel in air at 850？1,180 °C？？I: oxidation kinetics Oxid. Met. 2008 70 1？2 39 68 10.1007/s11085-008-9111-4

상세보기
50. Chen Y-T Biodegradation ZK50 magnesium alloy compression screws: mechanical properties, biodegradable characteristics and implant test J. Orthopaedic Sci. 2020 25 1107 1115 10.1016/j.jos.2020.01.018

상세보기
51. Li W In vitro and in vivo studies on ultrafine-grained biodegradable pure Mg, Mg？Ca alloy and Mg？Sr alloy processed by high-pressure torsion Biomater. Sci. 2020 8 18 5071 5087 10.1039/D0BM00805B 32812545

상세보기
52. Sikora-Jasinska M Synthesis, mechanical properties and corrosion behavior of powder metallurgy processed Fe/Mg2Si composites for biodegradable implant applications Mater. Sci. Eng. C 2017 81 511 521 10.1016/j.msec.2017.07.049

상세보기
53. Zumdick NA Additive manufactured WE43 magnesium: a comparative study of the microstructure and mechanical properties with those of powder extruded and as-cast WE43 Mater. Charact. 2019 147 384 397 10.1016/j.matchar.2018.11.011

상세보기
54. Hufenbach J Effect of selective laser melting on microstructure, mechanical, and corrosion properties of biodegradable FeMnCS for implant applications Adv. Eng. Mater. 2020 22 10 2000182 10.1002/adem.202000182

상세보기
55. Hermawan H Iron？manganese: new class of metallic degradable biomaterials prepared by powder metallurgy Powder Metall. 2008 51 1 38 45 10.1179/174329008X284868

상세보기
56. Yang Y A combined strategy to enhance the properties of Zn by laser rapid solidification and laser alloying J. Mech. Behav. Biomed. Mater. 2018 82 51 60 10.1016/j.jmbbm.2018.03.018 29567530

상세보기
57. Deng Q Fabrication of high-strength Mg？Gd？Zn？Zr alloy via selective laser melting Mater. Charact. 2020 165 110377 10.1016/j.matchar.2020.110377

상세보기
58. Lejcek P Selective laser melting of pure iron: Multiscale characterization of hierarchical microstructure Mater. Charact. 2019 154 222 232 10.1016/j.matchar.2019.05.012

상세보기
59. Thijs L A study of the microstructural evolution during selective laser melting of Ti？6Al？4V Acta Mater. 2010 58 9 3303 3312 10.1016/j.actamat.2010.02.004

상세보기
60. Amato KN Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting Acta Mater. 2012 60 5 2229 2239 10.1016/j.actamat.2011.12.032

상세보기
61. Guan K Effects of processing parameters on tensile properties of selective laser melted 304 stainless steel Mater. Des. 2013 50 581 586 10.1016/j.matdes.2013.03.056

상세보기
62. Thijs L Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder Acta Mater. 2013 61 5 1809 1819 10.1016/j.actamat.2012.11.052

상세보기
63. Song B Fabrication and microstructure characterization of selective laser-melted FeAl intermetallic parts Surf. Coat. Technol. 2012 206 22 4704 4709 10.1016/j.surfcoat.2012.05.072

상세보기
64. Callister DW Jr Materials Science and Engineering an Introduction 2000 5 Wiley
65. Harwood, J. Strengthening Mechanisms in Solids . in Metals Park: ASM Seminar . (1960).
66. Chen C Precipitation hardening of high-strength low-alloy steels by nanometer-sized carbides Mater. Sci. Eng. A 2009 499 1？2 162 166 10.1016/j.msea.2007.11.110

상세보기
67. Baker R Brandon D Nutting J The growth of precipitates Phil. Mag. 1959 4 48 1339 1345 10.1080/14786435908233369

상세보기
68. Lee W-B Carbide precipitation and high-temperature strength of hot-rolled high-strength, low-alloy steels containing Nb and Mo Metall. Mater. Trans. A. 2002 33 6 1689 10.1007/s11661-002-0178-2

상세보기
69. Rodrigues TA In-situ strengthening of a high strength low alloy steel during wire and arc additive manufacturing (WAAM) Addit. Manuf. 2020 34 101200
70. Ganeev AV On the nature of high-strength state of carbon steel produced by severe plastic deformation IOP Conf. Ser. Mater. Sci. Eng. 2014 63 012128 10.1088/1757-899X/63/1/012128

상세보기
71. Krielaart GP Zwaag S Kinetics of γ → α phase transformation in Fe？Mn alloys containing low manganese Mater. Sci. Technol. 2013 14 1 10 18 10.1179/mst.1998.14.1.10

상세보기
72. Song B Integral method of preparation and fabrication of metal matrix composite: selective laser melting of in-situ nano/submicro-sized carbides reinforced iron matrix composites Mater. Sci. Eng. A 2017 707 478 487 10.1016/j.msea.2017.09.092

상세보기
73. Kostryzhev A Comparative effect of Mo and Cr on microstructure and mechanical properties in NbV-microalloyed bainitic steels Metals 2018 8 2 134 10.3390/met8020134

상세보기
74. Misra RDK Ultrahigh strength hot rolled microalloyed steels: microstructural aspects of development Mater. Sci. Technol. 2013 17 9 1119 1129 10.1179/026708301101511040

상세보기
75. Sha W Development of structural steels with re resistant microstructures Mater. Sci. Technol. 2013 18 3 319 325 10.1179/026708301225000789

상세보기
76. International, A. ASTM E8/E8M-09 Standard Test Methods for Tension Testing of Metallic Materials . ASTM, (2011).
77. Toby BH Von Dreele RB GSAS-II: the genesis of a modern open-source all purpose crystallography software package J. Appl. Crystallogr. 2013 46 2 544 549 10.1107/S0021889813003531

상세보기
78. James JD A review of measurement techniques for the thermal expansion coefficient of metals and alloys at elevated temperatures Meas. Sci. Technol. 2001 12 3 R1 R15 10.1088/0957-0233/12/3/201

상세보기
79. Huang EW Element effects on high-entropy alloy vacancy and heterogeneous lattice distortion subjected to quasi-equilibrium heating Sci. Rep. 2019 9 1 14788 10.1038/s41598-019-51297-4 31616021

상세보기

LOADING...

활용도 분석정보

상세보기

다운로드

내보내기

활용도 Top5 논문

해당 논문의 주제분야에서 활용도가 높은 상위 5개 콘텐츠를 보여줍니다.
더보기 버튼을 클릭하시면 더 많은 관련자료를 살펴볼 수 있습니다.

표제어: PCR

동의어: Packet Collision Rate

용어 설명 출처 목록 (6)

용어 설명: PCR은 세균 특이성이 있는 primer를 이용하여 적은 수의 세균이 있을지라도 쉽게 검출할 수 있는 유용한 방법이며, 이를 이용하여 구강 내 치면세균막이나 타액에서 직접 세균을 검출할 수 있게 되었다[8].

내보내기 구분	파일저장 인쇄 메일전송
구성항목	기본정보 상세정보 관리번호, 논문명, 저널/프로시딩명, 저자 , 발행년, 권, 호, 시작페이지, 끝페이지, 발행기관 관리번호, 논문명, 대등논문명, 저자 , 저널/프로시딩명, 발행기관, 발행년, 발행언어, 권, 호, 시작페이지, 끝페이지, ISBN, ISSN, 주제분야, 키워드, 초록(한글), 초록(영문), 저자(소속기관)
저장형식	Text(ASCII format) Excel format RefWorks Direct Export RIS format (for Reference Manager, ProCite, EndNote), Scholar's Aids, Mendeley
메일정보	받는사람 (필수) @ 보내는사람 (선택) @ 제목 내용 KISTI 검색결과 이메일 서비스
안내	총 건의 자료가 검색되었습니다. 다운받으실 자료의 인덱스를 입력하세요. (1-10,000) 검색결과의 순서대로 최대 10,000건 까지 다운로드가 가능합니다. 데이타가 많을 경우 속도가 느려질 수 있습니다.(최대 2~3분 소요) 다운로드 파일은 UTF-8 형태로 저장됩니다. 파일의 내용이 제대로 보이지 않을실 때는 웹브라우저 상단의 보기 -> 인코딩 -> 자동선택 여부를 확인하십시오. ~ Text(ASCII format) Excel format

연합인증