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Inorganic chemistry, v.51 no.24, 2012년, pp.13162 - 13170
Dong, Qingsong (State Key Laboratory for Oxo Synthesis & Selective Oxidation, Lanzhou Institute of Chemical Physics, CAS, Lanzhou 730000, China) , Zhao, Yanxia (State Key Laboratory for Oxo Synthesis & Selective Oxidation, Lanzhou Institute of Chemical Physics, CAS, Lanzhou 730000, China) , Su, Yuanting (State Key Laboratory for Oxo Synthesis & Selective Oxidation, Lanzhou Institute of Chemical Physics, CAS, Lanzhou 730000, China) , Su, Ji-Hu (Hefei National Laboratory for Physical Sciences at Microscale and Department of Modern Physics, University of Science and Technology of China, Hefei 230026, China) , Wu, Biao (State Key Laboratory for Oxo Synthesis & Selective Oxidation, Lanzhou Institute of Chemical Physics, CAS, Lanzhou 730000, China) , Yang, Xiao-Juan (State Key Laboratory for Oxo Synthesis & Selective Oxidation, Lanzhou Institute of Chemical Physics, CAS, Lanzhou 730000, China)
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Reaction of L0NiBr2 with 2 equiv of NaH yielded the NiII hydride complex [(L•–)Ni(μ-H)2Ni(L•–)] (1) (L = [(2,6-iPr2C6H3)NC(Me)]2; L0 represents the neutral ligand, L•– is its radical-anionic form, and L2– denotes the dianion) in good yield. Stepwise reductio...
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