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Zeitschrift für physikalische Chemie, v.227 no.4, 2013년, pp.357 - 370
Gurentsov, Evgeny , Priemchenko, Konstantin , Grimm, Helge , Orthner, Hans , Wiggers, Hartmut , Borchers, Christine , Jander, Helga , Eremin, Alexander , Schulz, Christof
AbstractUnusually small carbon nanoparticles were synthesized in a microwave plasma flow-reactor by pyrolysis of 0.3–1.2% CH4, C2H4, and C2H2with 0.3–3.6% addition of molecular hydrogen in argon. Final particle sizes were analyzed by in-line particle-mass spectrometry (PMS) and by transmission electron microscopy (TEM). TEM measurements of primary particle sizes were found to be in a good agreement with PMS data. The carbon particles formed in the plasma generated by a 2.45 GHz magnetron with an applied power of 180 W and a total pressure of 13 mbar have diameters of 4–6 nm. The type of hydrocarbon precursor and 0.3–3.6% of hydrogen addition did not noticeably influence the final particle sizes. The formation of such small particles is attributed to the low pressure and the comparably low operation power. This method of small carbon nanoparticles synthesis could be useful for the production of carbon black material, where large surface area is important.
Gonzalez-Aguilar, J, Moreno, M, Fulcheri, L. Carbon nanostructures production by gas-phase plasma processes at atmospheric pressure. Journal of physics. D, applied physics, vol.40, no.8, 2361-2374.
Frenklach, M., Kematick, R., Huang, D., Howard, W., Spear, K. E., Phelps, A. W., Koba, R.. Homogeneous nucleation of diamond powder in the gas phase. Journal of applied physics, vol.66, no.1, 395-399.
Chen, Z., den Engelsen, D., Bachmann, P. K., van Elsbergen, V., Koehler, I., Merikhi, J., Wiechert, D. U.. High emission current density microwave-plasma-grown carbon nanotube arrays by postdepositional radio-frequency oxygen plasma treatment. Applied physics letters, vol.87, no.24, 243104-.
Dato, Albert, Frenklach, Michael. Substrate-free microwave synthesis of graphene: experimental conditions and hydrocarbon precursors. New journal of physics, vol.12, no.12, 125013-.
Prepr. Pap.-Am. Chem. Soc. Div. Fuel Chem. Cho W. 181 49 2004
Bladh, H., Johnsson, J., Olofsson, N.E., Bohlin, A., Bengtsson, P.E.. Optical soot characterization using two-color laser-induced incandescence (2C-LII) in the soot growth region of a premixed flat flame. Proceedings of the Combustion Institute, vol.33, no.1, 641-648.
Roth, P., Hospital, A.. Design and test of a particle mass spectrometer (PMS). Journal of aerosol science, vol.25, no.1, 61-73.
Giesen, B., Wiggers, H., Kowalik, A., Roth*, P.. Formation of Si-nanoparticles in a microwave reactor: Comparison between experiments and modelling. Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, vol.7, no.1, 29-41.
Hitzbleck, Klemens, Wiggers, Hartmut, Roth, Paul. Controlled formation and size-selected deposition of indium nanoparticles from a microwave flow reactor on semiconductor surfaces. Applied physics letters, vol.87, no.9, 093105-.
Green, K.M., Borras, M.C., Woskov, P.P., Flores, G.J., Hadidi, K., Thomas, P.. Electronic excitation temperature profiles in an air microwave plasma torch. IEEE transactions on plasma science, vol.29, no.2, 399-406.
Hecht, C., Abdali, A., Dreier, T., Schulz, C.. Gas-Temperature Imaging in a Microwave-Plasma Nanoparticle-Synthesis Reactor Using Multi-Line NO-LIF Thermometry. Zeitschrift für physikalische Chemie, vol.225, no.11, 1225-1235.
Cardoso, R P, Belmonte, T, Keravec, P, Kosior, F, Henrion, G. Influence of impurities on the temperature of an atmospheric helium plasma in microwave resonant cavity. Journal of physics. D, applied physics, vol.40, no.5, 1394-1400.
Proc. Combust. Inst. Frenklach M. 1075 22 1988 10.1016/S0082-0784(89)80117-1
Calcote, H.F.. Mechanisms of soot nucleation in flames-A critical review. Combustion and flame, vol.42, 215-242.
10.1007/978-3-642-85167-4_26
Frenklach, M., Yuan, T., Ramachandra, M. K.. Soot formation in binary hydrocarbon mixtures. Energy & fuels : an American Chemical Society journal, vol.2, no.4, 462-480.
Proc. Combust. Inst. Knorre V. G. 2303 26 1996 10.1016/S0082-0784(96)80058-0
Proc. Combust. Inst. Gulder L. 2351 26 1996 10.1016/S0082-0784(96)80064-6
Proc. Combust. Inst. Frenklach M. 2285 26 1996 10.1016/S0082-0784(96)80056-7
Janzen, C., Kleinwechter, H., Knipping, J., Wiggers, H., Roth, P.. Size analysis in low-pressure nanoparticle reactors: comparison of particle mass spectrometry with in situ probing transmission electron microscopy. Journal of aerosol science, vol.33, no.6, 833-841.
Fuchs, N. A.. On the stationary charge distribution on aerosol particles in a bipolar ionic atmosphere. Geofisica pura e applicata = Pure and applied geophysics, vol.56, no.1, 185-193.
Frenklach, Michael. Reaction mechanism of soot formation in flames. Physical chemistry chemical physics : PCCP, vol.4, no.11, 2028-2037.
Vander Wal, Randy L., Yezerets, Aleksey, Currier, Neal W., Kim, Do Heui, Wang, Chong Min. HRTEM Study of diesel soot collected from diesel particulate filters. Carbon, vol.45, no.1, 70-77.
Köylü, Ü.Ö., Faeth, G.M.. Fractal and projected structure properties of soot aggregates. Combustion and flame, vol.100, no.4, 621-633.
Murr, L.E., Soto, K.F.. A TEM study of soot, carbon nanotubes, and related fullerene nanopolyhedra in common fuel-gas combustion sources. Materials characterization, vol.55, no.1, 50-65.
Hu, Laigui, Wang, Shaomin, Zhang, Binzhi, Zeng, Yuewu. Structural changes in soot particles induced by diode laser irradiation. Carbon, vol.44, no.9, 1725-1729.
Zhu, Weizhong, Miser, Donald E, Geoffrey Chan, W, Hajaligol, Mohammad R. HRTEM investigation of some commercially available furnace carbon blacks. Carbon, vol.42, no.8, 1841-1845.
Woiki, D., Giesen, A., Roth, P.. Time-resolved laser-induced incandescence for soot particle sizing during acetylene pyrolysis behind shock waves. Proceedings of the Combustion Institute, vol.28, no.2, 2531-2537.
Alfè, M., Apicella, B., Rouzaud, J.-N., Tregrossi, A., Ciajolo, A.. The effect of temperature on soot properties in premixed methane flames. Combustion and flame, vol.157, no.10, 1959-1965.
Aggadi, N., Arnas, C., Bénédic, F., Dominique, C., Duten, X., Silva, F., Hassouni, K., Gruen, D.M.. Structural and chemical characterisation of soot particles formed in Ar/H2/CH4 microwave discharges during nanocrystalline diamond film synthesis. Diamond and related materials, vol.15, no.4, 908-912.
Stefanovic, I, Kovacevic, E, Berndt, J, Winter, J. Hα emission in the presence of dust in an Ar-C2H2radio-frequency discharge. New journal of physics, vol.5, no.1, 39-39.
Fusselman, Steven P., Yasuda, Hirotsugu K.. Particle densities and non-equilibrium in a low-pressure argon plasma jet. Plasma chemistry and plasma processing, vol.14, no.3, 251-275.
Hassouni, K., Mohasseb, F., Bénédic, F., Lombardi, G., Gicquel, A.. Formation of soot particles in Ar/H2/CH4 microwave discharges during nanocrystalline diamond deposition: A modeling approach. Pure and applied chemistry. : Chimie pure et appliqueé, vol.78, no.6, 1127-1145.
Deschenaux, Ch, Affolter, A, Magni, D, Hollenstein, Ch, Fayet, P. Investigations of CH4, C2H2 and C2H4 dusty RF plasmas by means of FTIR absorption spectroscopy and mass spectrometry. Journal of physics. D, applied physics, vol.32, no.15, 1876-1886.
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