[논문]Synchrotron X-ray microdiffraction analysis of abnormally growing grains induced by indentation in Fe-3%Si steel

Kim, Tae-Young; Shim, Hyung-Seok; Kim, Seunggyu; Choi, Sungki; Na, Tae-Wook; Kwon, Dongil; Hwang, Nong-Moon

doi:10.1016/j.matchar.2019.109845

[해외논문] Synchrotron X-ray microdiffraction analysis of abnormally growing grains induced by indentation in Fe-3%Si steel

Materials characterization, v.156, 2019년, pp.109845 -

Kim, Tae-Young (Department of Materials Science and Engineering, Seoul National University) , Shim, Hyung-Seok (National Center for Standard Data, Korea Research Institute of Standards and Science) , Kim, Seunggyu (Samsung Electronics) , Choi, Sungki (Department of Materials Science and Engineering, Seoul National University) , Na, Tae-Wook (Gangwon Regional Division, Korea Institute of Industrial Technology) , Kwon, Dongil (Department of Materials Science and Engineering, Seoul National University) , Hwang, Nong-Moon (Department of Materials Science and Engineering, Seoul National University)

Abstract ▼ AI-Helper

Abstract The effect of indentation using hardness testers on abnormal grain growth (AGG) of non-Goss grains were studied in Fe-3%Si steel. The primary recrystallized specimen was locally deformed by indentation under loads of 0.01, 0.05, 0.1, 0.2, 0.5, 2, 3, 6, 12 and 18 kgf and then heated to 860 °C and held for 10 min for recrystallization or recovery. When these specimens were heated to 1080 °C, AGG of non-Goss grains occurred around the area deformed by indentation loaded above 0.1 kgf. One abnormally growing grain was observed in the specimen indented under the loads of 0.2, 0.5, 2, 3 and 6 kgf, whereas three and eight abnormally growing grains were observed respectively in the specimen indented under loads of 12 and 18 kgf. Analyses by synchrotron X-ray microdiffraction show that all abnormally growing grains had sub-boundaries with the misorientation angles below 0.6o whereas no matrix grain had sub-boundaries. Highlights Abnormal grain growth occurs around the area deformed by indentation. Synchrotron X-ray microdiffraction can analyze sub-boundaries. All abnormally growing grains that are induced by indentation has sub-boundaries. Sub-boundaries formed by indentation are responsible for AGG of non-Goss grains. Graphical abstract [DISPLAY OMISSION]

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[해외논문] Synchrotron X-ray microdiffraction analysis of abnormally growing grains induced by indentation in Fe-3%Si steel

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[해외논문] Synchrotron X-ray microdiffraction analysis of abnormally growing grains induced by indentation in Fe-3%Si steel

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