Method of producing a metal-containing single-phase composition
국가/구분
United States(US) Patent
등록
국제특허분류(IPC7판)
C01B-033/00
C03C-003/118
C03C-003/076
C03C-003/102
출원번호
US-0481859
(2002-05-23)
우선권정보
SE-0102214(2001-06-21)
국제출원번호
PCT/SE02/000984
(2002-05-23)
§371/§102 date
20031220
(20031220)
국제공개번호
WO03/000618
(2003-01-03)
발명자
/ 주소
Sundberg,Mats
Lindgren,Kjell
El Raghy,Tamer
Barsoum,Michael
출원인 / 주소
Sandvik AB
Drexel University
인용정보
피인용 횟수 :
6인용 특허 :
9
초록▼
A method of producing a single-phase composition Mn+ 1AzXn, primarily the production of the single-phase material Ti3SiC2, where n lies within a range of 0.8-3. 2, where z lies within a range of 0.8-1.2, where M is at least one metal taken from the group of metals Ti (titanium), Sc (scandium), V (v
A method of producing a single-phase composition Mn+ 1AzXn, primarily the production of the single-phase material Ti3SiC2, where n lies within a range of 0.8-3. 2, where z lies within a range of 0.8-1.2, where M is at least one metal taken from the group of metals Ti (titanium), Sc (scandium), V (vanadium), Cr (chromium), Zr (zirconium), Nb (niobium) and Ta (tantalum), where X is at least one of the non-metals C (carbon) and N nitrogen), and where A is at least one of the chemical elements Si (silicon), Al (aluminum) and Sn (tin) or a compound of those elements, such that the final, desired compound will include the components Mn+1A zXn. A powder mixture of the components is formed and is ignited under an inert atmosphere to prevent promotion of dissociation and to cause the components to react.
대표청구항▼
What is claimed is: 1. A method of producing a single-phase composition Mn+ 1AzXn, by means of SHS (Self-propagating High Temperature Synthesis), where n lies within a range of 0.8-3.2, where z lies within a range of 0.8-1.2, where component M is at least one metal selected from the group consistin
What is claimed is: 1. A method of producing a single-phase composition Mn+ 1AzXn, by means of SHS (Self-propagating High Temperature Synthesis), where n lies within a range of 0.8-3.2, where z lies within a range of 0.8-1.2, where component M is at least one metal selected from the group consisting of Ti (titanium), Sc (scandium), V (vanadium), Cr (chromium), Zr (zirconium) , Nb (niobium) and Ta (tantalum) , and where component X is at least one of the non-metals C (carbon) and N (nitrogen), and where component A is at least one of the chemical elements Si (silicon), Al (aluminum), and Sn (tin) or a compound containing at least one of said chemical elements, such that a final, desired compound will include the components Mn+1AzX n, said method comprising the steps of: forming a powder mixture from components M, X, and A; adding to the powder mixture a pre-reacted compound to provide a resulting mixture, the pre-reacted compound having the composition Mn+1AzX n and serving as a heat sink; reacting the resulting mixture by igniting said powder mixture under an inert atmosphere to prevent dissociation of a resulting single-phase composition; and maintaining the reaction temperature at or above a temperature at which the components react but below a temperature at which the resulting single-phase composition dissociates. 2. A method according to claim 1, wherein n ranges from 1 to 3. 3. A method according to claim 1, wherein the single-phase material is Ti3SiC2. 4. A method according to claim 1, wherein the single-phase material is at least one of Ti2AlC and Ti2SnC. 5. A method according to claim 1, wherein the pre-reacted material is present at about 25 weight-% of the mixed materials. 6. A method according to claim 5, wherein the pre-reacted material is Ti3SiC2. 7. A method according to claim 1, wherein the inert atmosphere has a partial pressure of oxygen sufficiently low to prevent dissociation of the single-phase composition.
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이 특허에 인용된 특허 (9)
Dunmead Stephen D. (Davis CA) Holt Joseph B. (San Jose CA) Kingman Donald D. (Danville CA) Munir Zuhair A. (Davis CA), Dense, finely, grained composite materials.
Dunmead Stephen D. (Davis CA) Holt Joseph B. (San Jose CA) Kingman Donald D. (Danville CA) Munir Zuhair A. (Davis CA), Grained composite materials prepared by combustion synthesis under mechanical pressure.
Gottselig Bernd (Frechen DEX) Gyarmati Ern (Jlich DEX) Naoumidis Aristides (Jlich DEX), Method and components for bonding a silicon carbide molded part to another such part or to a metallic part.
Shaw Karl G. (Troy NY) Alman David E. (Troy NY) Cooper RenM. (Ballston Spa NY) German Randall M. (State College PA) McCoy Kazuo P. (Troy NY), Process for making finely divided intermetallic.
Shaw Karl G. (Spring Avenue Extension Troy NY 12180) Alman David E. (212 River St. ; Apt. #3 Troy NY 12180) Cooper ReneM. (70 Frederick St. Ballston Spa NY 12020) German Randall M. (1145 Outer Dr. St, Process for producing finely divided intermetallic and ceramic powders and products thereof.
Gupta, Surojit; Palanisamy, Thirumalai G.; Barsoum, Michel; Li, Chien Wei, Ternary carbide and nitride materials having tribological applications and methods of making same.
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