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| 국가/구분 | United States(US) Patent 등록 |
|---|---|
| 국제특허분류(IPC7판) |
|
| 출원번호 | US-0443934 (2012-04-11) |
| 등록번호 | US-8741818 (2014-06-03) |
| 발명자 / 주소 |
|
| 출원인 / 주소 |
|
| 대리인 / 주소 |
|
| 인용정보 | 피인용 횟수 : 1 인용 특허 : 309 |
An embodiment includes a method of servicing a well bore. The method may comprise introducing a lost circulation composition into a lost circulation zone, the lost circulation composition comprising hydraulic cement, nano-particles, amorphous silica, clay, and water. The method further may comprise
An embodiment includes a method of servicing a well bore. The method may comprise introducing a lost circulation composition into a lost circulation zone, the lost circulation composition comprising hydraulic cement, nano-particles, amorphous silica, clay, and water. The method further may comprise allowing the lost circulation composition to set in the lost circulation zone. Another embodiment includes a lost circulation composition. The lost circulation may comprise hydraulic cement, nano-particles, amorphous silica, clay, and water.
1. A lost circulation composition comprising: hydraulic cement in an amount of about 0.1% to about 25% by weight of the lost circulation composition;nano-particles having a particle size in a range from about 1 nanometer to about 100 nanometers and present in an amount of about 0.1% to about 10% by
1. A lost circulation composition comprising: hydraulic cement in an amount of about 0.1% to about 25% by weight of the lost circulation composition;nano-particles having a particle size in a range from about 1 nanometer to about 100 nanometers and present in an amount of about 0.1% to about 10% by weight of the lost circulation composition, wherein the nano-particles comprise nano-particles selected from the group consisting of colloidal nano-silica, nano-alumina, nano-zinc oxide, nano-boron, nano-iron oxide, nano-calcium carbonate, and any combination thereof;amorphous silica in an amount of about 0.1% to about 15% by weight of the lost circulation composition;a nano-clay having a particle size in a range of from about 1 nanometer to about 100 nanometers and present in an amount of about 0.1% to about 2% by weight of the lost circulation composition; andwater in an amount of about 60% to about 80% by weight of the lost circulation composition;wherein the lost circulation composition has a 10-second static gel strength of at least about 15 lbf/100 ft2 at room temperature,wherein the lost circulation composition has a 10-minute static gel strength of at least about 25 lbf/100 ft2 at room temperature,wherein the lost circulation composition is a sealing composition that prevents the migration of fluids. 2. The lost circulation composition of claim 1 wherein the lost circulation composition has a consistency of less than 35 Bc at a temperature up to about 193° when under shear at 150 rpm, develops a consistency of greater than 70 Bc when the shear is stopped, and then thins to a consistency of less than 35 BC at a temperature up to about 193° F. when shear is re-applied at 150 rpm. 3. The lost circulation composition of claim 1 wherein the lost circulation composition has a density of about 6 pounds per gallon to about 14 pounds per gallon. 4. The lost circulation composition of claim 1 wherein the hydraulic cement comprises at least one hydraulic cement selected from the group consisting of a Portland cement, a pozzolana cement, a gypsum cement, a high-alumina-content cement, a slag cement, and any combination thereof. 5. The lost circulation composition of claim 1 wherein the nano-particles have a particle size of about 5 nanometers to about 50 nanometers. 6. The lost circulation composition of claim 1 wherein the nano-particles comprise the colloidal nano-silica. 7. The lost circulation composition of claim 1 wherein the nano-clay comprises a synthetic nano-clay. 8. The lost circulation composition of claim 1 wherein the nano-clay comprises a synthetic nano-clay, and wherein the nano-particles comprise the colloidal nano-silica. 9. The lost circulation composition of claim 1 wherein the lost circulation composition further comprises sub-micron sized calcium carbonate. 10. The lost circulation composition of claim 1 wherein the lost circulation composition further comprises at least one additive selected from the group consisting of a strength-retrogression additive, a set accelerator, a set retarder, a weighting agent, a lightweight additive, a gas-generating additive, a mechanical property enhancing additive, a lost-circulation material, a filtration-control additive, a dispersant, a fluid loss control additive, a defoaming agent, a foaming agent, a thixotropic additive, and any combination thereof. 11. The lost circulation composition of claim 1 wherein the lost circulation composition further comprises at least one additive selected from the group consisting of crystalline silica, fumed silica, salt, fiber, hydratable clay, calcined shale, vitrified shale, microsphere, fly ash, slag, diatomaceous earth, metakaolin, rice husk ash, natural pozzolan, zeolite, cement kiln dust, lime, elastomer, resin, latex, and any combination thereof. 12. A lost circulation composition comprising: hydraulic cement in an amount of about 0.1% to about 25% by weight of the lost circulation composition;nano-particles having a particle size in a range of from about 1 nanometer to about 100 nanometers and present in an amount of about 0.1% to about 10% by weight of the lost circulation composition, wherein the nano-particles comprise nano-particles selected from the group consisting of colloidal nano-silica, nano-alumina, nano-zinc oxide, nano-boron, nano-iron oxide, nano-calcium carbonate, and any combination thereof;amorphous silica in an amount of about 0.1% to about 15% by weight of the lost circulation composition;a nano-clay having a particle size in a range of from about 1 nanometer to about 100 nanometers and present in an amount of about 0.1% to about 2% by weight of the lost circulation composition; andwater in an amount of about 60% to about 80% by weight of the lost circulation composition;wherein the lost circulation composition has a density of about 6 pounds per gallon to about 14 pounds per gallon,wherein the lost circulation composition has a 10-second static gel strength of at least about 15 lbf/100 ft2 at room temperature,wherein the lost circulation composition has a 10-minute static gel strength of at least about 25 lbf/100 ft2 at room temperature,wherein the lost circulation composition is a sealing composition that prevents the migration of fluids. 13. The lost circulation composition of claim 12 wherein the lost circulation composition has a consistency of less than 35 Bc at a temperature up to about 193° when under shear at 150 rpm, develops a consistency of greater than 70 Bc when the shear is stopped, and then thins to a consistency of less than 35 BC at a temperature up to about 193° F. when shear is re-applied at 150 rpm. 14. The lost circulation composition of claim 12 wherein the hydraulic cement comprises at least one hydraulic cement selected from the group consisting of a Portland cement, a pozzolana cement, a gypsum cement, a high-alumina-content cement, a slag cement, and any combination thereof. 15. The lost circulation composition of claim 12 wherein the nano-particles have a particle size of about 5 nanometers to about 50 nanometers. 16. The lost circulation composition of claim 12 wherein the nano-particles comprise the colloidal nano-silica. 17. The lost circulation composition of claim 12 wherein the nano-clay comprises a synthetic nano-clay. 18. The lost circulation composition of claim 12 wherein the lost circulation composition further comprises sub-micron sized calcium carbonate. 19. The lost circulation composition of claim 12 wherein the lost circulation composition further comprises at least one additive selected from the group consisting of a strength-retrogression additive, a set accelerator, a set retarder, a weighting agent, a lightweight additive, a gas-generating additive, a mechanical property enhancing additive, a lost-circulation material, a filtration-control additive, a dispersant, a fluid loss control additive, a defoaming agent, a foaming agent, a thixotropic additive, and any combination thereof. 20. The lost circulation composition of claim 12 wherein the lost circulation composition further comprises at least one additive selected from the group consisting of crystalline silica, fumed silica, salt, fiber, hydratable clay, calcined shale, vitrified shale, microsphere, fly ash, slag, diatomaceous earth, metakaolin, rice husk ash, natural pozzolan, zeolite, cement kiln dust, lime, elastomer, resin, latex, and any combination thereof. 21. A lost circulation composition comprising: Portland cement in an amount of about 10% to about 20% by weight of the lost circulation composition;colloidal nano-silica in an amount of about 0.5% to about 4% by weight of the lost circulation composition, the colloidal nano-silica having a particle size of about 1 nanometer to about 100 nanometers;amorphous silica in an amount of about 5% to about 10% by weight of the lost circulation composition;synthetic nano-clay in an amount of about 0.5% to about 2% by weight of the lost circulation composition; andwater in an amount of about 60% to about 75% by weight of the lost circulation composition,wherein the lost circulation composition has a 10-second static gel strength of at least about 15 lbf/100 ft2 at room temperature,wherein the lost circulation composition has a 10-minute static gel strength of at least about 25 lbf/100 ft2 at room temperature,wherein the lost circulation composition is a sealing composition that prevents the migration of fluids. 22. The lost circulation composition of claim 21 wherein the lost circulation composition has a consistency of less than 35 Bc at a temperature up to about 193° when under shear at 150 rpm, develops a consistency of greater than 70 Bc when the shear is stopped, and then thins to a consistency of less than 35 BC at a temperature up to about 193° F. when shear is re-applied at 150 rpm. 23. The lost circulation composition of claim 21 wherein the lost circulation composition further comprises sub-micron sized calcium carbonate. 24. The lost circulation composition of claim 21 wherein the lost circulation composition further comprises at least one additive selected from the group consisting of a strength-retrogression additive, a set accelerator, a set retarder, a weighting agent, a lightweight additive, a gas-generating additive, a mechanical property enhancing additive, a lost-circulation material, a filtration-control additive, a dispersant, a fluid loss control additive, a defoaming agent, a foaming agent, a thixotropic additive, and any combination thereof. 25. The lost circulation composition of claim 21 wherein the lost circulation composition further comprises at least one additive selected from the group consisting of crystalline silica, fumed silica, salt, fiber, hydratable clay, calcined shale, vitrified shale, microsphere, fly ash, slag, diatomaceous earth, metakaolin, rice husk ash, natural pozzolan, zeolite, cement kiln dust, lime, elastomer, resin, latex, and any combination thereof. 26. The lost circulation composition of claim 21 wherein the lost circulation composition has a density of about 6 pounds per gallon to about 14 pounds per gallon. 27. The lost circulation composition of claim 21 wherein the lost circulation composition comprises sub-micron sized calcium carbonate in an amount of about 15% to about 50% by weight of the hydraulic cement.
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