Equal temperature distillation chamber and method
원문보기
IPC분류정보
국가/구분
United States(US) Patent
등록
국제특허분류(IPC7판)
B01D-003/32
B01D-005/00
B01J-019/30
출원번호
US-0668177
(2017-08-03)
등록번호
US-9895626
(2018-02-20)
발명자
/ 주소
Kremerman, Elliot
출원인 / 주소
Kremerman, Elliot
대리인 / 주소
Feigin, Esq., Michael J.
인용정보
피인용 횟수 :
2인용 특허 :
28
초록▼
An equal temperature fractional distillation chamber allows for more precise distillation by providing solid particulate matter with air spaces, such as Raschig rings, to radiate heat from the bottom of the chamber to an area where the vapors are separated. This area is unencumbered by Raschig rings
An equal temperature fractional distillation chamber allows for more precise distillation by providing solid particulate matter with air spaces, such as Raschig rings, to radiate heat from the bottom of the chamber to an area where the vapors are separated. This area is unencumbered by Raschig rings or other devices and can be reduced in size, as necessary, to be less than 20% or 10% of the vertical height of the chamber. Further, a distillation key can enter from the top of the chamber and come down into the chamber with rings which encourage condensation of vapors which rise upwards. In this manner, a very controlled and accurate distillation can be achieved due to the higher heat capacity of the glass or other materials around the unencumbered region.
대표청구항▼
1. A distillation head, comprising: a vertically extending inner chamber extending between a lower portal and an upper portal with a pinched inner region in a lower section of said inner chamber;a plurality of Raschig rings above, and supported by, said pinched inner region of said vertically extend
1. A distillation head, comprising: a vertically extending inner chamber extending between a lower portal and an upper portal with a pinched inner region in a lower section of said inner chamber;a plurality of Raschig rings above, and supported by, said pinched inner region of said vertically extending inner chamber;a hollow portion of said vertically extending inner chamber between said Raschig rings and a side portal, said side portal connecting said hollow portion of said vertically extending inner chamber with a hollow portion of a discharge chamber;said upper portal being centered with respect to said side walls and sealed by way of a distillation key which extends into said inner chamber which is entirely centered with respect to said side walls. 2. The distillation head of claim 1, further comprising: a distillation key extending within a single said upper portal of said vertically extending inner chamber towards said Raschig rings which is equi-spaced from side walls of said vertically extending inner chamber, said side walls being walls extending between said upper portal and said lower portal of said vertically extending inner chamber. 3. The distillation head of claim 2, wherein a portion of said vertically extending inner chamber unencumbered by either said distillation key and said Raschig rings is heated by a heat source below said bottom portal and is of substantially equal temperature to said Raschig rings. 4. The distillation head of claim 2, wherein a portion of said vertically extending inner chamber unencumbered by either said distillation key and said Raschig rings comprises less than 20% of a vertical distance of said vertically extending inner chamber. 5. The distillation head of claim 1, wherein said vertically extending inner chamber is at least mostly surrounded by an air-tight enclosed jacket having two spaced apart layers and shared airspace with a portal extending between and opening into said two layers which is transverse to said vertically extending inner chamber. 6. The distillation head of claim 1, wherein said vertically extending inner chamber and said pinched inner region are formed together as one continuous and uninterrupted unit of inert glass material; a continuous and uninterrupted vertical region extends from below said pinched region, through said pinched region, and above said pinched region, said uninterrupted vertical region passing through said pinched region being more narrow than any of said plurality of Raschig rings;and said pinched region has rounded inner side walls. 7. A method of using the distillation head of claim 3, comprising: placing said plurality of Raschig rings through said upper portal before melting a solid such that it's vapors extend upwards from said bottom portal, between said Raschig rings, and at least partially out of said side portal. 8. The method of using the distillation head of claim 7, wherein said vapors, when between said bottom portal and said unencumbered portion of said vertically extending chamber are of substantially the same temperature, said same temperature being elevated at least 50 degrees Celsius over ambient air temperature. 9. The distillation head of claim 1, wherein said distillation key has a plurality of spaced apart rings positioned below said side portal which extend horizontally from a solid body of said distillation key. 10. A fractional distillation device comprising: an unencumbered mid-region of a vertical chamber;a plurality of Raschig rings extending from said unencumbered mid-region to a narrowest section of said vertical chamber;a centered top portal adapted for passage there-through of said pluraly of Raschig rings and wider than said narrowest section;wherein said vertical chamber comprises a bottom portal below said narrowest region, a top portal on a side opposite said bottom portal, and side portal opening into said vertical chamber above said unencumbered region. 11. The fractional distillation device of claim 10, further comprising an upper region having a horizontally centered key extending downwards from said top portal of said vertical chamber, said upper region being defined as between said top portal and a lowest extent of said key. 12. The fractional distillation device of claim 10, further comprising a double layered airtight jacket around at least a majority of said upper region and said unencumbered mid-region of said vertical chamber. 13. The fractional distillation device of claim 12, further comprising a portal between each layer of said double layered airtight jacket. 14. The fractional distillation device of claim 12, calibrated such that heated vapors which extend from beneath said device into said vertical chamber through said bottom portal and at least partially out of said side portal cause a constant temperature or substantially constant temperature to be reached, over time, between said bottom portal and said unencumbered mid-region. 15. The fractional distillation device of claim 14, wherein said substantially constant temperature is further in an entirety of said unencumbered region. 16. A method of fractional distillation of matter which comprises solids at room temperature, comprising the steps of: placing Raschig rings through an upper portal in a vertical chamber of a fractional distillation device, said vertical chamber having a portion thereof uninterrupted by solid material between a bottom most extent of said device, said vertical chamber being narrowed at sides thereof;continuing to place said Raschig rings into said vertical chamber until said Raschig rings reach at least a height of an airtight jacket;heating a solid beneath said vertical chamber causing at least some vapors from said solid to pass, without prior blockage, directly through and above said Raschig rings and exit through a side portal of said vertical chamber, said side portal being above said Raschig rings;wherein a temperature of said vapors passing through said Raschig rings as well as between said Raschig rings and said side portals are of substantially the same temperature throughout a majority of said fractional distillation. 17. The method of fractional distillation of claim 16, wherein said airtight jacket is double layered. 18. The method of fractional distillation of claim 17, wherein a portal extends between each layer of said double layered said airtight jacket. 19. The method of fractional distillation of claim 16, further comprising, before said step of heating, placing a distillation key into an upper portal of said vertical chamber such that said distillation key extends a majority of a distance between said upper portal and an upper extent of said Raschig rings. 20. The method of fractional distillation of claim 19, where said same temperature extends to a bottom most extent of said distillation key.
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