Processes for recovering products from a corn fermentation mash
원문보기
IPC분류정보
국가/구분
United States(US) Patent
등록
국제특허분류(IPC7판)
C12P-007/14
C12P-019/02
C12P-019/14
출원번호
US-0604507
(2017-05-24)
등록번호
US-10059966
(2018-08-28)
발명자
/ 주소
Bootsma, Jason
출원인 / 주소
Flint Hills Resources, LP
인용정보
피인용 횟수 :
0인용 특허 :
17
초록▼
Processes and systems for recovering products from a fermentation mash. In some examples, a process for recovering products from a fermentation mash can include processing a ground corn product to produce a fermentation mash that can include ethanol. At least a portion of the ethanol can be separate
Processes and systems for recovering products from a fermentation mash. In some examples, a process for recovering products from a fermentation mash can include processing a ground corn product to produce a fermentation mash that can include ethanol. At least a portion of the ethanol can be separated from the fermentation mash to produce a whole stillage. The whole stillage can be separated to produce a fiber rich product and a filtrate. The fiber rich product can be hydrolyzed to produce a saccharification mash. The saccharification mash can be processed to produce additional ethanol and a stillage protein product.
대표청구항▼
1. A process for recovering products from a fermentation mash, comprising: processing a ground corn product to produce a fermentation mash comprising ethanol;separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;separating the whole stillage to produce a
1. A process for recovering products from a fermentation mash, comprising: processing a ground corn product to produce a fermentation mash comprising ethanol;separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;separating the whole stillage to produce a fiber rich product and a filtrate;hydrolyzing the fiber rich product to produce a saccharification mash; andprocessing the saccharification mash to produce additional ethanol and a stillage protein product comprising about 15 wt % to about 35 wt % of yeast, based on a dry weight of the stillage protein product. 2. The process of claim 1, wherein the stillage protein product comprises about 20 wt % to about 30 wt % of the yeast, based on the dry weight of the stillage protein product. 3. The process of claim 1, wherein the stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product. 4. The process of claim 1, wherein the stillage protein product further comprises protein, fat, ash, neutral detergent fibers, and acid detergent fibers, and wherein the stillage protein product comprises about 47 wt % to about 57 wt % of the protein, about 3 wt % to about 5 wt % of the fat, about 1 wt % to about 3 wt % of the ash, about 4 wt % to about 10 wt % of the neutral detergent fibers, about 5 wt % to about 10 wt % of the acid detergent fibers, and about 20 wt % to about 30 wt % of the yeast, based on the dry weight of the stillage protein product. 5. The process of claim 1, wherein the fiber rich product has an ethanol potential of at least 90 gallons of ethanol per 1,000 kilograms of the fiber rich product. 6. The process of claim 1, wherein the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product. 7. The process of claim 1, wherein greater than 80 wt % of the ground corn product has a particle size of 425 μm or less, as measured according to AOAC 965.22-1966. 8. The process of claim 1, wherein the fiber rich product is contacted with an acid or a base prior to hydrolyzing the fiber rich product to produce the saccharification mash. 9. The process of claim 1, wherein: greater than 80 wt % of the ground corn product has a particle size of 425 μm or less, as measured according to AOAC 965.22-1966,the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product,the fiber rich product is contacted with an acid or a base prior to hydrolyzing the fiber rich product to produce the saccharification mash, andthe stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product. 10. A process for recovering products from a fermentation mash, comprising: processing a ground corn product to produce a fermentation mash comprising ethanol;separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;separating the whole stillage with a fiber filter to produce a fiber rich product and a filtrate;hydrolyzing the fiber rich product to produce a saccharification mash; andprocessing the saccharification mash to produce additional ethanol and a stillage protein product comprising about 15 wt % to about 35 wt % of yeast, based on a dry weight of the stillage protein product. 11. The process of claim 10, wherein the fiber filter comprises a filter sleeve having openings of about 10 μm to less than 400 μm. 12. The process of claim 10, wherein the fiber filter comprises a filter sleeve and a rotor disposed within the filter sleeve, and wherein the filter sleeve comprises a woven polymer fabric. 13. The process of claim 10, wherein the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product. 14. The process of claim 10, wherein the stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product. 15. The process of claim 10, wherein the stillage protein product further comprises protein, fat, ash, neutral detergent fibers, and acid detergent fibers, and wherein the stillage protein product comprises about 47 wt % to about 57 wt % of the protein, about 3 wt % to about 5 wt % of the fat, about 1 wt % to about 3 wt % of the ash, about 4 wt % to about 10 wt % of the neutral detergent fibers, about 5 wt % to about 10 wt % of the acid detergent fibers, and about 20 wt % to about 30 wt % of the yeast, based on the dry weight of the stillage protein product. 16. The process of claim 10, wherein: the fiber filter comprises a filter sleeve having openings of about 10 μm to less than 400 μm,the fiber rich product has an ethanol potential of at least 90 gallons of ethanol per 1,000 kilograms of the fiber rich product, andthe stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product. 17. A process for recovering products from a fermentation mash, comprising: processing a ground corn product to produce a fermentation mash comprising ethanol;separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;separating the whole stillage to produce a fiber rich product and a filtrate, wherein the fiber rich product has an ethanol potential of at least 90 gallons of ethanol per 1,000 kilograms of the fiber rich product,hydrolyzing the fiber rich product to produce a saccharification mash;processing the saccharification mash to produce additional ethanol and a stillage protein product comprising about 15 wt % to about 35 wt % of yeast, based on a dry weight of the stillage protein product, andseparating the filtrate to produce a protein rich portion, an oil product, and a clarified stillage. 18. The process of claim 17, wherein the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product. 19. The process of claim 17, wherein the fiber rich product has an ethanol potential of about 135 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product. 20. The process of claim 17, wherein greater than 80 wt % of the ground corn product has a particle size of 425 μm or less, as measured according to AOAC 965.22-1966. 21. The process of claim 17, wherein the whole stillage is separated with a fiber filter to produce the fiber rich product and the filtrate, and wherein the fiber filter comprises a filter sleeve having openings of about 10 μm to about 400 μm. 22. The process of claim 17, further comprising: removing water from the protein rich portion to produce a protein rich product; andremoving water from the clarified stillage to produce an evaporated clarified stillage. 23. The process of claim 5, wherein the whole stillage is separated with a fiber filter to produce the fiber rich product and a filtrate.
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