초록

메조포어를 갖는 분자체의 합성
. 계면활성제에 따른 메조포어 분자체의 설계 및 합성경로 탐구
. 고 비표면적을 갖는 메조포어 분자체의 제조
. 제조된 물질의 특성 분석
. 응용을 위한 기초 반응실험

Abstract ▼

The recent synthesis of silica-based mesoporous materials by the cooperative assembly of perioctic inorganic and surfactant-based structures has attracted great interest because'it extends the range of molecular-sieve materials into the very-large-pore regime. There is no doubt that the synthesis of

The recent synthesis of silica-based mesoporous materials by the cooperative assembly of perioctic inorganic and surfactant-based structures has attracted great interest because'it extends the range of molecular-sieve materials into the very-large-pore regime. There is no doubt that the synthesis of these materials opens definitive new possibilities for preparing catalysts with uniform pores in the mesoporous region, which should importantly allow the relatively large molecules present in crude oils and in the production of fine chemicals to be reacted. Obviously when a new type of materials such as these are . ctiscovered, an explosion of scientific and commercial development swiftly follows, and new investigations on every conceivable aspect of their nature, the synthesis procedures and synthesis mechanisms, heteroatom insertion, characterization, adsorption, and catalytic properties, rapidly occurs.
The objective of this research which is the first year research for the study on the synthesis and application of mesoporous molecular sieve is a development of the synthesis method of mesoporous molecular sieve.

목차 Contents

• 제 1 장 서 론...15
• 제 2 장 기술현황...19
• 제 1 절 배경...19
• 제 2 절 합성이론...26
• 제 3 장 실 험...46
• 제 1 절 메조포어 분자체의 제조...46
• 제 2 절 메조포어 분자체의 특성분석...51
• 제 3 절 반응 실험...52
• 제 4 장 결과 및 고찰...56
• 제 1 절 MCM-41의 합성 및 특성분석...56
• 제 2 절 MCM-48의 합성 조건 고찰...62
• 제 3 절 특성 분석...90
• 제 4 절 반응성...96
• 제 5 장 결 론...98
• 참고문헌...99