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Macromolecular symposia, v.296 no.1, 2010년, pp.626 - 631
Tischler, Christian (Department of Plastics Technology and Environmental Engineering, Federal Testing Centre &ndash) , Kratochvilla, Thomas R. (TGM, Wexstraß) , Muschik, Heinz (e 19‐) , Dragaun, Heinz (23, A‐)
AbstractSummary: It is known, that the lifetime of polyethylene pipes is essentially limited by slow crack growth (SCG). For state of the art PE materials common SCG testing methods have reached their limits with respect to extension of testing times. A comparatively new method is the Notched Ring Test (NRT) as developed by Choi et al.[1] Pipe rings notched at the inner wall are used. The test is carried out in 80 °C water under constant bending load. The arrangement of the notch at the inner wall reduces testing times using the residual stress of extruded pipes. A disadvantage of this method is that there is no clearly defined failure time because SCG takes place between two phases of creeping. The output of this test is an “on‐set slow cracking time” (crack initiation), obtained by analysis of the displacement curve. In this work it has been shown that the NRT method yields to brittle fracture within acceptable time frames.[2] Methods for data analysis are presented. This test could be very useful applied in research and development for resin evaluation and as a tool in quality control in pipe production for evaluating the process conditions.
1 S. Choi , S. Pyo , Y. S. Suh , Y. Seo , Development of notched ring test for measuring slow cracking resistance in plastics pipes and fittings Plastics , Rubber and Composites 2007 , 36 ( 4 ) 219 – 225 (7).
2 Ch. Tischler , Development and Verification of a New Plastics Pipes Test Method for Slow Crack Growth Determination, Diplomarbeit, Institut für Festkörperphysik der TU‐Wien, 2008 .
3 ISO 16770 (2004‐02‐01), Plastics ‐ Determination of the environmental stress cracking (ESC) of polyethylene ‐ Full‐notch creep test (FNCT).
4 ISO 16241 (2005‐02‐15), Notch tensile test to measure the resistance to slow crack growth of polyethylene materials for pipe an fitting products (PENT).
5 ISO 13479 (1997‐05‐01) 'Polyolefin pipes for the conveyance of fluids ‐ Determination of resistance to crack propagation ‐ Test method for slow crack growth on notched pipes (notch test).
6 R. Carlos Corleto , Accelerated method to determine or predict failure in polyethylene , Plastics Pipes XIII, Washington 2006 .
7 S. Choi , et al. Development of standard test method for slow crack growth determination of plastic materials by cyclic fatigue loading , Hannam University , Daejeon 2008 .
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