[보고서]조선왕조실록 밀랍본의 가온가압 탈랍처리기술 연구

조병묵

보고서 정보

주관연구기관

강원대학교 산학협력단
Kangwon National University

연구책임자

조병묵

참여연구자

강규영 , 조병욱 , 유원재 , 김혁중 , 최도침 , 이한솔 , 최은연

보고서유형

최종보고서

발행국가

대한민국

언어

한국어

발행년월

2010-12

과제시작연도

2010

주관부처

문화재청

사업 관리 기관

국립문화재연구소

등록번호

TRKO201200010626

과제고유번호

1555000343

사업명

보존복원기술개발연구

DB 구축일자

2013-04-18

키워드

조선왕조실록 밀랍본.복원.탈랍.보강.안전성.The beeswax-treated Annals of Joseon Dynasty.restoration.dewaxing.strengthening.safety.

표 Sheet producing factors of test Hanji
표 Microchamber and preparation of VOCs test.
표 Experimental conditions of micro chamber
표 Analysis conditions for TD-GC/MS
표 Experimental set-up to study the effect of VOCs from beeswax.
표 Standard sugar solutions
표 HPLC conditions for monomeric carbohydrate determination
표 Dionex ICS-3000 and autosampler.
표 List of mechanical strength test methods and testers
표 Test methods and items for optical properties of Hanji
표 Elrepho spectrophotometer.
표 Effect of dry heat aging on beeswax
표 Effect of dry heat aging at 150℃ on weight loss of beeswax.
표 Effect of dry heat aging at 150℃ on acid value of beeswax.
표 Effect of dry heat aging at 150℃ on IR spectra of beeswax.
표 Effect of dry heat aging at 150℃ on oxidation index of beeswax.
표 Comparison of IR spectra of beeswax and dewaxed Hanji.
표 Comparison of IR spectra of beeswax and dewaxed Hanji aged at 150℃ for 1 day.
표 Comparison of IR spectra of beeswax and dewaxed Hanji aged at 150℃ for 2 days.
표 Comparison of IR spectra of beeswax and dewaxed Hanji aged at 150℃ for 3 days.
표 Effect of dry heat aging at 150℃ on IR spectra of beeswax-treated Hanji.
표 Effect of dry heat aging at 120℃ on weight loss of Hanji.
표 Effect of dry heat aging at 120℃ on optical properties of Hanji
표 Effect of dry heat aging at 120℃ on brightness of Hanji.
표 Effect of dry heat aging at 120℃ on L* value of Hanji.
표 Effect of dry heat aging at 120℃ on strength properties of Hanji
표 Effect of dry heat aging at 120℃ on a* and b* values of Hanji.
표 Effect of dry heat aging at 120℃ on folding endurance.
표 Effect of dry heat aging at 120℃ on tensile strength.
표 Effect of dry heat aging at 120℃ on elongation of Hanji.
표 Effect of dry heat aging at 120℃ on zero-span tensile strength.
표 Effect of dry heat aging at 120℃ on viscosity of pulp.
표 Effect of dry heat aging at 120℃ on pH of hot and cold extracts of Hanji.
표 Effect of dry heat aging at 120℃ on IR spectra of Hanji.
표 Effect of dry heat aging at 120℃ on oxidation index.
표 VOCs derived from beeswax
표 Chromatogram of the VOCs from beeswax at 65℃.
표 Effect of dry heat aging at 150℃ on tensile strength of Hanji, Hanji with beeswax and beeswax-treated Hanji in bal direction.
표 Effect of dry heat aging at 150℃ on tensile strength of Hanji, Hanji with beeswax and beeswax-treated Hanji in cross bal direction.
표 Effect of dry heat aging at 150℃ on tensile index of Hanji, Hanji with beeswax and beeswax-treated Hanji in bal direction.
표 Effect of dry heat aging at 150℃ on tensile index of Hanji, Hanji with beeswax and beeswax-treated Hanji in cross bal direction
표 Effect of dry heat aging at 150℃ on elongation of Hanji, Hanji with beeswax and beeswax-treated Hanji in bal direction.
표 Effect of dry heat aging at 150℃ on elongation of Hanji, Hanji with beeswax and beeswax-treated Hanji in cross bal direction.
표 Effect of dry heat aging at 150℃ on tensile energy absorption (TEA) of Hanji, Hanji with beeswax and beeswax-treated Hanji in bal direction.
표 Effect of dry heat aging at 150℃ on tensile energy absorption (TEA) of Hanji, Hanji with beeswax and beeswax-treated Hanji in cross bal direction.
표 Effect of dry heat aging at 150℃ on folding endurance of Hanji, Hanji with beeswax and beeswax-treated Hanji in bal direction.
표 Effect of dry heat aging at 150℃ on folding endurance of Hanji, Hanji with beeswax and beeswax-treated Hanji in bal direction.
표 Effect of dry heat aging at 150℃ on zero span tensile strength of Hanji and Hanji with beeswax.
표 Effect of dry heat aging at 150℃ on viscosity of Hanji, Hanji with beeswax, and beeswax-treated Hanji.
표 Comparison of FT-IR spectra of Hanji and beeswax-treated Hanji as the control.
표 Effect of dry heat aging at 150℃ on IR spectra of Hanji.
표 Effect of dry heat aging at 150℃ on IR spectra of Hanji with beeswax..
표 Effect of dry heat aging at 150℃ on IR spectra of beeswax-treated Hanji.
표 Effect of dry heat aging at 150℃ on oxidation index.
표 Effect of dry heat aging at 150℃ on carboxyl content.
표 Effect of dry heat aging at 150℃ on pH of cold and hot water extracts.
표 Effect of dewaxing treatment by heat & pressure on viscosity of Hanji
표 Effect of pressing temperature of hot plate on viscosity of Hanji
표 Effect of dewaxing treatment by heat & pressure on carboxyl content of Hanji
표 Sugar contents of dewaxed Hanji by dewaxing treatment by heat & pressure
표 Effect of pressure and temperature of supercritical CO2 extraction on viscosity of Hanji.
표 Effect of pressure and temperature of supercritical CO2 extraction on viscosity of Hanji
표 Sugar contents of dewaxed Hanji by supercritical CO2 extraction
표 Effect of type of strengthening agent on dry heat aging of dewaxed Hanji
표 Effect of type of strengthening agent on viscosity of cellulose during dry heat aging at 150℃..
표 Effect of type of strengthening agent on viscosity reduction during dry heat aging at 150℃.
표 Supercritical carbon dioxide extraction apparatus.
표 Experimental conditions
표 Variation of solubility depend on pressure and temperature in supercritical fluid.
표 High pressure soxhlet apparatus.
표 Beeswax-treated Hanji before and after treatment of SFE.
표 Beeswax-treated Hanji before and after treatment of SFE depends on temperature and pressure as extraction operating parameters.
표 Dewaxing yield depends on temperature and pressure.
표 Dewaxing yield depends on temperature and pressure
표 Variation of density of dewaxed Hanji.
표 Variation of density of dewaxed Hanji
표 Variation of physical properties
표 Variation of folding endurance.
표 Variation of tensile strength.
표 Variation of tensile index.
표 Variation of TEA.
표 Variation of dewaxing yield depends on CO2 flow rate and CO2 consumption.
표 Variation of dewaxing yield depends on CO2 flow rate and CO2 consumption
표 Extracted beeswax (yellow beeswax & white beeswax).
표 DSC analysis of waxes.
표 Conditions of GC analysis
표 Chemical composition of waxes.
표 Extracted solution by SFE using ethanol as a co-solvent.
표 Ethanol solution of extracts by ethanol extraction with sonication.
표 Solubility test of beeswaxes in ethanol. [ Original beeswax(left), extracted yellow beeswax(middle), extracted white beeswax(right) ]
표 Variation of physical properties of samples treated by SFE with ethanol as a co-solvent
표 Variation of folding endurance.
표 Variation of tensile strength.
표 Variation of tensile index.
표 Variation of TEA.
표 FT-IR analysis of dewaxed Hanji.
표 SEM images of dewaxed Hanji (×200)
표 Preservation test of ink on aged beeswax Hanji after treatment of SFE.
표 Variation of chromaticity of ink on aged beeswax Hanji after treatment of SFE.
표 Preservation test of ink on aged beeswax Hanji after ethanol extraction with sonication.
표 Dewaxed Hanji after treatment of high pressure soxhlet.
표 Amount of extracted beeswax depends on CO2 consumption
표 Amount of extracted beeswax depends on CO2 consumption.
표 Ink-printed Hanji before and after treatment of SFE repeated 6 times.
표 Ink-printed Hanji before and after treatment of ethanol with sonication.
표 Sheet making factors of Hanji
표 Basic information of Hanji
표 The image of auto bar coater set up hot plate for preparation of beeswax-treated Hanji.
표 Operation conditions of auto bar coater
표 The image of hot press for the dewaxing treatment of beeswax-treated Hanji.
표 The image of vacuum chamber for the dewaxing treatment of beeswax-treated Hanji.
표 Oven dryer for aging test.
표 Image of scanning electron microscope (SEM).
표 Test methods for measurement of mechanical properties
표 Folding endurance tester.
표 Zero-span tensile strength tester.
표 Tensile strength tester.
표 Test methods for measurement of optical properties
표 Spectrophotometer of Elrepho type.
표 Image of ATR-IR for measurement of oxidation index and crystallinity index.
표 Changes in folding endurance (1 kgf) of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours. (bal cross direction : ⊥, bal direction : ∥)
표 Changes in folding endurance (1 kgf) of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours.
표 Changes in tensile strength of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours. (bal cross direction : ⊥, bal direction : ∥)
표 Changes in tensile strength of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours
표 Changes in tensile energy absorption of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours. (bal cross direction : ⊥, bal direction : ∥)
표 Changes in TEA of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours
표 Changes in zero-span tensile strength of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours. (bal cross direction : ⊥, bal direction : ∥)
표 Changes in zero-span tensile strength of beeswax-treated Hanji after accelerated aging at 150℃ during 48 hours
표 Changes in L value of beeswax-treated Hanji after accelerated aging at 150℃ during 72 hours.
표 Changes in a and b value of beeswax-treated Hanji after accelerated aging at 150℃ during 72 hours.
표 Changes in brightness of beeswax-treated Hanji after accelerated aging at 150℃ during 72 hours.
표 Changes in yellowness of beeswax-treated Hanji after accelerated aging at 150℃ during 72 hours.
표 Changes in oxidation index of beeswax-treated Hanji after accelerated aging at 150℃ during 72 hours.
표 Changes in crystallinity index of beeswax-treated Hanji after accelerated aging at 150℃ during 72 hours.
표 The dewaxing ratio of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in density of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Dewaxing ratio of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 150℃, 12 MPa, 10 times treatment).
표 Changes in density of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 150 ℃, 12 MPa, 10 times treatment).
표 SEM images of Hanji, beeswax-treated Hanji, 24 hours aged beeswax-treated Hanji (×200).
표 SEM images of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions (×200).
표 Changes in folding endurance of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in folding endurance of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions
표 Changes in tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions
표 Changes in tensile energy absorption of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in tensile energy absorption of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions
표 Changes in zero-span tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in zero-span tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in folding endurance (0.5 kgf) of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in folding endurance (0.5 kgf) of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment)
표 Changes in tensile index of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in tensile index of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment)
표 Changes in zero-span tensile index of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in zero-span tensile index of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment)
표 Changes in L value of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in a value of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in b value of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in brightness of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in yellowness of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in L value of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in a value of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in b value of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in yellowness of beeswax-treated Hanji treated with accelerated aging treatment at 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in yellowness of beeswax-treated Hanji treated with accelerated aging treatmentat 150℃ during 72 hours (dewaxing condition : 100℃, 12 MPa, 10 times treatment).
표 Changes in oxidation index of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 Changes in crystallinity index of beeswax-treated Hanji according to the dewaxing times under different heat-pressure sensitive conditions.
표 The results of folding endurance for evaluation of aging safety of dewaxed Hanji.
표 The results of folding endurance for evaluation of aging safety of dewaxed Hanji
표 The results of tensile index for evaluation of aging safety of dewaxed Hanji.
표 The results of tensile index for evaluation of aging safety of dewaxed Hanji
표 The results of zero-span tensile index for evaluation of aging safety of dewaxed Hanji.
표 The results of zero-span tensile index for evaluation of aging safety of dewaxed Hanji
표 The results of L value for evaluation of aging safety of dewaxed Hanji.
표 The results of a value for evaluation of aging safety of dewaxed Hanji.
표 The results of b value for evaluation of aging safety of dewaxed Hanji.
표 The results of brightness for evaluation of aging safety of dewaxed Hanji.
표 The results of yellowness for evaluation of aging safety of dewaxed Hanji.
표 The results of oxidation index for evaluation of aging safety of dewaxed Hanji.
표 The results of crystallinity index for evaluation of aging safety of dewaxed Hanji.
표 The dewaxing ratio of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in folding endurance (0.5 kgf) of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in folding endurance (0.5 kgf) of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions
표 Changes in tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions
표 Changes in zero-span tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in zero-span tensile index of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions
표 Changes in L value of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in a value of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in b value of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in brightness of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Changes in yellowness of beeswax-treated Hanji according to the dewaxing times under different heat-suction sensitive conditions.
표 Change in mechanical properties of Hanji and beeswax-treated Hanji according to the moist heat treatment at different temperature and 50% relative humidity.
표 Change in optical properties of Hanji and beeswax-treated Hanji according to the moist heat treatment at different temperature and 50% relative humidity.
표 Change in chemical properties of Hanji and beeswax-treated Hanji according to the moist heat treatment at different temperature and 50% relative humidity.
표 Equation of oxidation index according to the moist heat treatment at different temperature and 50% relative humidity
표 Calculation of k value according to the moist heat treatment at different temperature and 50% relative humidity
표 Arrhenius plots of rate constants of degradation for Hanji and beeswax-treated Hanji.
표 The paper making conditions of Hanji
표 Kinds of natural and synthetic polymer for reinforcement
표 Dipping method of Hanji.
표 Dipping method of aged and dewaxed Hanji.
표 Coating method of Hanji.
표 Dewaxing method of beeswax treated Hanji.
표 Measurements of varius sample
표 Tensile strength tester.
표 Elmendorf tear strength tester.
표 MIT folding endurance tester.
표 FE-SEM.
표 ATR-IR spectrometer and analysis method of samples.
표 Tensile index of aged Hanji.
표 Tensile loss of aged Hanji.
표 Tear index of aged Hanji.
표 Tear loss of aged Hanji.
표 Logarithm of Folding endurance of Fig.
표 Strength and standard deviation of tensile, tear index and folding endurance of aged Hanji
표 Folding endurance loss of aged Hanji.
표 Treated weight of polymer treated Hanji with reinforcing treatment method.
표 Tensile index of polymer treated Hanji with reinforcing treatment method.
표 Logarithm of folding endurance of polymer treated Hanji with reinforcing treatment method.
표 Coating weight of natural polymer treated Hanji.
표 Coating weight of synthetic polymer treated Hanji.
표 Tensile index of natural polymer treated Hanji.
표 Tensile index of synthetic polymer treated Hanji.
표 Tear index of natural polymer treated Hanji.
표 Tear index of synthetic polymer treated Hanji.
표 Logarithm of folding endurance of synthetic natural polymer treated Hanji.
표 Logarithm of folding endurance of polymer treated Hanji.
표 Strength and standard deviation of tensile, tear index and folding endurance of polymer treated Hanji
표 Coating weight of polymer treated aged Hanji.
표 Tensile index of natural polymer treated aged Hanji.
표 Tensile index of synthetic polymer treated aged Hanji.
표 The rate charge in tensile index after 48 hr aging.
표 Tear index of natural polymer treated aged Hanji.
표 Tear index of synthetic polymer treated aged Hanji.
표 The rate charge in tear index after 48hr aging.
표 Logarithm of folding endurance of natural polymer treated aged Hanji.
표 Logarithm of folding endurance of synthetic polymer treated aged Hanji.
표 The rate charge in folding endurance after 48hr aging.
표 Strength and standard deviation of tensile, tear index and folding endurance of polymer treated aged Hanji
표 IR spectra of Hanji and 48 hr aged Hanji.
표 Oxidation index of Hanji and 48 hr aged Hanji.
표 IR spectra of CMC treated aged Hanji.
표 Oxidation index of CMC treated aged Hanji.
표 R spectra of EC treated aged Hanji.
표 Oxidation index of EC treated aged Hanji.
표 IR spectra of MC treated aged Hanji.
표 Oxidation index of MC treated aged Hanji.
표 IR spectra of PVA 1500 treated aged Hanji.
표 Oxidation index of PVA 1500 treated aged Hanji.
표 IR spectra of PVA 2000 treated aged Hanji.
표 Oxidation index of PVA 2000 treated aged Hanji.
표 IR spectra of PEG 1500 treated aged Hanji.
표 Oxidation index of PEG 1500 treated aged Hanji.
표 FE-SEM images of Hanji.
표 FE-SEM images of 48 hr aged Hanji.
표 FE-SEM images of CMC treated aged Hanji (0 hr).
표 FE-SEM images of CMC treated aged Hanji (48 hr).
표 FE-SEM images of MC treated aged Hanji (0 hr).
표 FE-SEM images of MC treated aged Hanji (12 hr).
표 FE-SEM images of MC treated aged Hanji (24 hr).
표 FE-SEM images of MC treated aged Hanji (36 hr).
표 FE-SEM images of MC treated aged Hanji (48 hr).
표 Tensile strength of various polymer treated dewaxed Hanji.
표 Tensile index of various polymer treated dewaxed Hanji.
표 Tear index of various polymer treated various dewaxed Hanji.
표 Logarithm of folding endurance of polymer treated dewaxed Hanji.
표 Tensile index of natural polymer treated dewaxed Hanji.
표 Tensile index of synthetic polymer treated dewaxed Hanji.
표 Tensile loss of natural polymer treated treated dewaxed Hanji.
표 Tensile loss of synthetic polymer dewaxed Hanji.
표 Tear index of natural polymer treated dewaxed Hanji.
표 Tear index of synthetic polymer treated dewaxed Hanji.
표 Tear loss of natural polymer treated dewaxed Hanji.
표 Tear loss of synthetic polymer treated dewaxed Hanji.
표 Logarithm of folding endurance of synthetic natural polymer treated dewaxed Hanji.
표 Logarithm of folding endurance of polymer treated dewaxed Hanji.
표 Folding endurance loss of natural polymer treated dewaxed Hanji.
표 Folding endurance loss of synthetic polymer treated dewaxed Hanji.
표 Tensile index of MC treated dewaxed MC Hanji(heat&press).
표 Comparison to tensile index of two treated dewaxed Hanji.
표 Disparity of tensile index of two MC treated dewaxed Hanji.
표 Tear index of MC treated dewaxed Hanji (heat & press).
표 Comparison to tear index of two MC treated dewaxed Hanji.
표 Disparity of tear index of two MC treated dewaxed Hanji.
표 Logarithm of folding endurance of MC treated dewaxed Hanji (heat & press).
표 Comparison to folding endurance of two MC treated dewaxed Hanji.
표 Disparity of folding endurance of two MC treated dewaxed Hanji.

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조선왕조실록 밀랍본의 가온가압 탈랍처리기술 연구
Studies on dewaxing techniques for restoration of the beeswax-treated Annals of Joseon Dynasty 원문보기

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조선왕조실록 밀랍본의 가온가압 탈랍처리기술 연구 Studies on dewaxing techniques for restoration of the beeswax-treated Annals of Joseon Dynasty 원문보기

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조선왕조실록 밀랍본의 가온가압 탈랍처리기술 연구
Studies on dewaxing techniques for restoration of the beeswax-treated Annals of Joseon Dynasty 원문보기

표/그림 (287)

표/그림 (287)