[논문]Comparison of the Cold-Pressed Peel Oil Composition between ]Korean and Japanese Satsuma Mandarin (Citrus unshiu Marcov. forma Miyagawa-wase) by GC, GC-MS and GC-O

Park, Hyang-Sook; Sawamura, Masayoshi

doi:10.3746/jfn.2002.7.1.005

Comparison of the Cold-Pressed Peel Oil Composition between ]Korean and Japanese Satsuma Mandarin (Citrus unshiu Marcov. forma Miyagawa-wase) by GC, GC-MS and GC-O 원문보기

Journal of food science and nutrition, v.7 no.1, 2002년, pp.5 - 11

Park, Hyang-Sook (Department of Food Nutrition, Shinheung College) , Sawamura, Masayoshi (Department of Bioresources Science, Faculty of Agriculture, Kochi University)

Abstract ▼ AI-Helper

The comparison of the volatile flavor components from Korean and Japanese Satsuma mandarin (C. unshiu Marcov. forma Miyagawa-wase) peel oils, isolated by cold-pressing, was performed by gas chromatography, mass-spectrometry and gas chromatography-olfactometry (GC-O). Eighty-five volatile components were identified in each oil by GC and GC-MS. Forty-three components were detected in each oil by GC-O. The total amount of monoterpene hydrocarbons was 95.88% (Korean mandarin) and 95.29% (Japanese mandarin). Limonene, ${\gamma}$-terpinene, myrcene and $\alpha$-pinene were the main components of the cold-pressed oils from the both samples. The volatile composition of the Japanese mandarin was characterized by a higher content of sesquiterpene hydrocarbons, especially bicyclogermacrene, $\alpha$-humullene and valencene. The volatile composition of two samples can easily be distinguished by the percentages of aldehydes, ketones and esters, which were found at higher levels in the Japanese mandarin. The sweet and fruity flavor was stronger in the Korean mandarin oil while herbaceous flavor was stronger in Japanese sample. From GC-O data it is suggested that the sweet and fruity flavor of the Korean mandarin resulted from terpinolene and linalool, and the herbaceous note of the Japanese mandarin from $\alpha$-humullene, nepal, ι-carvone and perill aldehyde.

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문제 정의

A number of factors including climate, genetics, soil conditions are involved in determining citrus oil quality. The objective of this study was to investigate the differences of cold-pressed peel oil composition between Korean and Japanese Satsuma mandarin, miyagawa wase unshiu.

제안 방법

components detected. The analysis was carried out on a Shimadzu GC-17A linked with a Shimadzu QP-5000 at a MS ionization voltage of 70 eV, accelerating voltage of 1500 V, and ion source temperature of 250℃. The GC column and oven conditions were the same as those given above for the GC-14A.

대상 데이터

A Shimadzu GC-14A gas chromatograph(GC) equipped with a DB-Wax fused-silica capillary column (60me×0.25mm i. d., film thickness 0.25μm, J & W Scientific, Folsom, CA, USA) and a flame ionization detector(FID) was used. Peak areas were integrated with a Shimadzu C-R6A Chromatopack integrator.
Eleven ester components were confirmed in mandarin oils. Esters are usually almost absent from Citrus oil, but various ester components were found in this study.
Satsuma mandarin (Citrus unshiu Marcov. forma Miyagawa-wase), which were harvested in November 2000, were provided by the Citrus Experiment Station Rural Development Administration, Jeju, Korea, and the Kochi Prefectural Fruit Tree Experimental Station, Kochi, Japan, respectively. The climates between Jeju of Korea and Kochi Prefectures of Japan are similar.
01%) found in at low levels. Seven kinds of oxides and 3 kinds of acids were found in this study. The content of rrane-linalool fur anoxide was higher in Korean mandarin whereas cis-linalool pyranoxide was shown vise versa.

이론/모형

The oil samples from Korean and Japanese mandarin were prepared according to the cold-pressing method described by Sawamura and Kuriyama(14). The fruits were sliced and the mesocarp and albedo layers were peeled off from the flavedo.

성능/효과

32% of the oil from the Korean-grown mandarin. The difference between Korean and Japanese mandarins with regard to the weight percentage of aldehydes could be due to octanal (Korean mandarin; 0.06%, Japanese mandarin; 0.11%), neral(0.09%, 0.16%), dodecanal(0.04%, 0.11%), trans-2-undecenal(0.07%, 0.18%) and perill aldehyde(0.02%, 0.09%).

참고문헌 (23)

Baker, C. M. Ann, Manwell, Clyde. Molecular genetics of avian proteins : I. The egg white proteins of the domestic fowl. British poultry science, vol.3, no.3, 161-174.

상세보기
Kraft, Monica, Vianna, Elcio, Martin, Richard J., Leung, Donald Y.M.. Nocturnal asthma is associated with reduced glucocorticoid receptor binding affinity and decreased steroid responsiveness at night. The Journal of allergy and clinical immunology : official organ of American Academy of Allergy, vol.103, no.1, 66-71.

상세보기
Besler, M., Steinhart, H., Paschke, A.. Allergenicity of hen's egg‐white proteins: IgE binding of native and deglycosylated ovomucoid. Food and agricultural immunology, vol.9, no.4, 277-288.

상세보기
Kume, Tamikazu, Matsuda, Tsukasa. Changes in structural and antigenic properties of proteins by radiation. Radiation physics and chemistry, vol.46, no.2, 225-231.

상세보기
Smith, P.K., Krohn, R.I., Hermanson, G.T., Mallia, A.K., Gartner, F.H., Provenzano, M.D., Fujimoto, E.K., Goeke, N.M., Olson, B.J., Klenk, D.C.. Measurement of protein using bicinchoninic acid. Analytical biochemistry, vol.150, no.1, 76-85.

상세보기
Lee, Ju.-Woon, Yook, Hong.-Sun, Lee, Kyong.-Haeng, Kim, Jae.-Hun, Kim, Woo.-Jung, Byun, Myung.-Woo. Conformational changes of myosin by gamma irradiation. Radiation physics and chemistry, vol.58, no.3, 271-277.

상세보기
CHAN, J.K., GILL, T.A., PAULSON, A.T.. Thermal Aggregation of Myosin Subfragments from Cod and Herring. Journal of food science : an official publication of the Institute of Food Technologists, vol.58, no.5, 1057-1061.

상세보기
LAEMMLI, U. K.. Cleavage of Structural Proteins during the Assembly of the Head of Bacteriophage T4. Nature, vol.227, no.5259, 680-685.

상세보기
Claeys, E., Uytterhaegen, L., Buts, B., Demeyer, D.. Quantification of beef myofibrillar proteins by SDS-PAGE. Meat science, vol.39, no.2, 177-193.

상세보기
Kume, Tamikazu, Ishii, Tetsuya, Matsuda, Tsukasa. Immunochemical identification of irradiated chicken eggs. Journal of the science of food and agriculture, vol.65, no.1, 1-4.

상세보기
FILALI-MOUHIM , M. AUDETTE, M. ST-LOUIS, L. THAUVETTE, L. DENOROY , F. PENIN*, X. CHEN, N. ROULEAU, J.-P. LE CAER , J. ROSSIER*, M. POTIER and M. LE MAIRE, A.. Lysozyme fragmentation induced by gamma-radiolysis. International journal of radiation biology, vol.72, no.1, 63-70.

상세보기
Samejima, Kunihiko, Lee, Nam H, Ishioroshi, Makoto, Asghar, Ali. Protein extractability and thermal gel formability of myofibrils isolated from skeletal and cardiac muscles at different post‐mortem periods. Journal of the science of food and agriculture, vol.58, no.3, 385-393.

상세보기
Horowits, Robert, Kempner, Ellis S., Bisher, Margaret E., Podolsky, Richard J.. A physiological role for titin and nebulin in skeletal muscle. Nature, vol.323, no.6084, 160-164.

상세보기
VAJDI, M., PEREIRA, R. R.. COMPARATIVE EFFECTS OF ETHYLENE OXIDE, GAMMA IRRADIATION AND MICROWAVE TREATMENTS ON SELECTED SPICES. Journal of food science : an official publication of the Institute of Food Technologists, vol.38, no.5, 893-895.

상세보기
Stachowicz, Waclaw, Strzelczak‐Burlinska, Grazyna, Michalik, Jacek, Wojtowicz, Andrzej, Dziedzic‐Goclawska, Anna, Ostrowski, Kazimierz. Application of electron paramagnetic resonance (EPR) spectroscopy for control of irradiated food. Journal of the science of food and agriculture, vol.58, no.3, 407-415.

상세보기
IINO, Kyuei, OSODO, Kazuo. Evaluation of Edible Quality of Commercail Satsuma mandarin (Citrus unshiu MARC.). 園藝學會雜誌 = Journal of the Japanese Society for Horticultural Science, vol.41, no.4, 398-404.

상세보기
OSODO, Kazuo, IINO, Kyuei. Evaluation of Edible Quality of Commercial Satsuma Mandarin (Citrus unshiu Marc.). 園藝學會雜誌 = Journal of the Japanese Society for Horticultural Science, vol.41, no.1, 83-91.

상세보기
MAOTANI, Toru, KAWASE, Kenji, KAMURO, Yasuo, HIRAI, Koichi. Effects of Ethylene on Peel Puffing of Satsuma Mandarin. 園藝學會雜誌 = Journal of the Japanese Society for Horticultural Science, vol.52, no.3, 238-242.

상세보기
KITAGAWA, Hirotoshi, TARUTANI, Takayuki. Studies on the Coloring of Satsuma Mandarin (Citrus unshiu MARC.). 園藝學會雜誌 = Journal of the Japanese Society for Horticultural Science, vol.42, no.1, 65-69.

상세보기
Sawamura, Masayoshi, Kuriyama, Toshinao. Quantitative determination of volatile constituents in the pummelo (Citrus grandis Osbeck forma Tosa-buntan). Journal of agricultural and food chemistry, vol.36, no.3, 567-569.

상세보기
10.1002/(SICI)1099-1026(199605)11:3 3.0.CO;2-O

상세보기
Ravid, Uzi, Putievsky, Eli, Katzir, Irena. Determination of the enantiomeric composition of α‐terpineol in essential oils. Flavour and fragrance journal, vol.10, no.4, 281-284.

상세보기
Choi, H.-S., Sawamura, M.. Composition of the Essential Oil of Citrus tamurana Hort. ex Tanaka (Hyuganatsu). Journal of agricultural and food chemistry, vol.48, no.10, 4868-4873.

상세보기

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