[논문]Effect of various intraoral repair systems on the shear bond strength of composite resin to zirconia

Han, In-Hae; Kang, Dong-Wan; Chung, Chae-Heon; Choe, Han-Cheol; Son, Mee-Kyoung

doi:10.4047/jap.2013.5.3.248

Effect of various intraoral repair systems on the shear bond strength of composite resin to zirconia 원문보기

The journal of advanced prosthodontics, v.5 no.3, 2013년, pp.248 - 255

Han, In-Hae (Department of Prosthodontics, School of Dentistry, Chosun University) , Kang, Dong-Wan (Department of Prosthodontics, School of Dentistry, Chosun University) , Chung, Chae-Heon (Department of Prosthodontics, School of Dentistry, Chosun University) , Choe, Han-Cheol (Department of Dental Materials, School of Dentistry, Chosun University) , Son, Mee-Kyoung (Department of Prosthodontics, School of Dentistry, Chosun University)

Abstract ▼ AI-Helper

PURPOSE. This study compared the effect of three intraoral repair systems on the bond strength between composite resin and zirconia core. MATERIALS AND METHODS. Thirty zirconia specimens were divided into three groups according to the repair method: Group I-CoJet$^{TM}$ Repair System (3M ESPE) [chairside silica coating with $30{\mu}m$ $SiO_2$ + silanization + adhesive]; Group II-Ceramic Repair System (Ivoclar Vivadent) [etching with 37% phosphoric acid + Zirconia primer + adhesive]; Group III-Signum Zirconia Bond (Heraus) [Signum Zirconia Bond I + Signum Zirconia Bond II]. Composite resin was polymerized on each conditioned specimen. The shear bond strength was tested using a universal testing machine, and fracture sites were examined with FE-SEM. Surface morphology and wettability after surface treatments were examined additionally. The data of bond strengths were statistically analyzed with one-way ANOVA and Tamhane post hoc test (${\alpha}$=.05). RESULTS. Increased surface roughness and the highest wettability value were observed in the CoJet sand treated specimens. The specimens treated with 37% phosphoric acid and Signum Zirconia Bond I did not show any improvement of surface irregularity, and the lowest wettability value were found in 37% phosphoric acid treated specimens. There was no significant difference in the bond strengths between Group I ($7.80{\pm}0.76$ MPa) and III ($8.98{\pm}1.39$ MPa). Group II ($3.21{\pm}0.78$ MPa) showed a significant difference from other groups (P<.05). CONCLUSION. The use of Intraoral silica coating system and the application of Signum Zirconia Bond are effective for increasing the bond strength of composite resin to zirconia.

주제어

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문제 정의

trength between composite resin and zirconia. Intraoral silica coating system used in this study represents a feasible method for improving zirconia surface roughness and wettability. However, the presence of MDP and methyl methacrylate in the Signum Zirconia Bond may increase the bond strength by the formation of chemical bonds between composite resin and zirconia.

제안 방법

Therefore, the purpose of this in vitro study was to evaluate the effect of 3 different intraoral repair systems on the shear bond strength of composite resin to zirconia.
To simulate this clinical condition, all specimens were ground using a fine-grit diamond rotary cutting instrument (Red stripe round-end straight diamond bur, 30 μm grit size; Komet®, Germany) in a high-speed handpiece with water irrigation for 10 seconds.

대상 데이터

The specimens were airborne-particle, abraded using a chairside abrader (Ultra- Blaster, Ultradent Products Inc., USA) for 15 seconds with 30 μm silica-modified Al2O3 particles (CoJetTM) with 3.0 bar pressure from 10 mm distance.
ulser, Milan, Italy). The specimens were treated with a bifunctional methacrylate based component containing acetone and MDP (Signum Zirconia Bond I and dried with oilfree air. A bonding agent containing methyl methacrylate and diphenyl (2,4,6-trimethylbenzoyl) phosphinoxide (Signum Zirconia Bond II) was then applied to the zirconia surface with a disposable brush and light-cured for 40 seconds.
Thirty zirconia specimens (10 mm × 10 mm × 2 mm) were produced by a CAD/CAM system (Zirkonzahn, Italy) using prefabricated blocks of zirconia (Prettau Zircon; Zirkonzahn, Italy) and then sintered according to the manufacturer’s instructions.
Zirconia specimens were embedded in liquid unsaturated polyester (EPOVIA® RF-9000, Cray valley Inc., Korea) (Fig. 1).

데이터처리

Results of the shear bond test were statistically analyzed with one-way ANOVA (SPSS 15.0, SPSS Inc., Chicago, IL, USA), followed by a Tamhane post hoc test (α=.05).

성능/효과

34°). Particularly, the contact angle value after CoJet sand treatment in Group I was measured to be noticeably lowers than those of other groups; thus excellent surface wettability was shown (Fig. 4).

후속연구

y storing specimens at 37℃ for 72 hours. As further studies, the change of bond strength after long-term storage as well as thermal cycling treatments is required. And also, the comparison of the bond strength after repeated fatigue loadings is required additionally.

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