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Determination of pectolinarin in Cirsium spp. using HPLC/UV analysis 원문보기

Journal of applied biological chemistry, v.59 no.2, 2016년, pp.107 - 112  

Cho, Sunghun (Department of Integrative Plant Science, Chung-Ang University) ,  Lee, Jaemin (Department of Integrative Plant Science, Chung-Ang University) ,  Lee, Yoon Kyoung (Department of Integrative Plant Science, Chung-Ang University) ,  Chung, Mi Ja (Department of Food Science and Nutrition, Gwangju University) ,  Kwon, Ki Han (Department of Food Science and Nutrition, Gwangju University) ,  Lee, Sanghyun (Department of Integrative Plant Science, Chung-Ang University)

Abstract ▼ AI-Helper 아이콘AI-Helper

Pectolinarin was isolated from the ethyl acetate fraction of Cirsium setidens using open column chromatography and was analyzed using spectrometry. Pectolinarin content in Cirsium spp. was determined using HPLC/UV. Pectolinarin content in the aerial part of Cirsium spp. was higher than that in the r...

주제어

#Cirsium spp   #   #Flavonoid   #High-performance liquid chromatography   #Pectolinarin  

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대상 데이터

  • LEE 2014-02) were deposited at the Herbarium of Department of Integrative Plant Science, ChungAng University, Republic of Korea. Cirsium extracts, including the aerial parts of C. setidens, C. nipponicum, and C. chanroenicum, and the roots of C. chanroenicum, were obtained from the Plant Extract Bank of Korea Research Institute of Bioscience and Biotechnolgy in Deajeon, Korea. Extracts from the aerial parts of C.
  • Chemical shifts are reported in parts per million (δ), and coupling constants (J) are expressed in hertz. The HPLC system consisted of a WATERS 1525 Binary HPLC (Milford, MA, USA), a TCM column oven, and a WATERS 2489 UV/visible detector, all controlled by a computer using Empower Pro 2.0 software. The separation column was a Waters Spherisorb® INNO column C18 (4.
  • maackii was obtained from Department of Herbal Crop Research, National Institute of Horticultural & Herbal Science, RDA, Eumseong, Republic of Korea. Voucher specimens (C. setidens, No. LEE 2014-01; C. japonicum var. maackii, No. LEE 2014-02) were deposited at the Herbarium of Department of Integrative Plant Science, ChungAng University, Republic of Korea. Cirsium extracts, including the aerial parts of C.
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참고문헌 (24)

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  2. Ganzera M, Pocher A, Stuppner H (2005) Differentiation of Cirsium japonicum and C. setosum by TLC and HPLC-MS. Phytochem Anal 16(3): 205-209 

    상세보기 crossref

  3. Jeong DM, Jung HA, Choi JS (2008) Comparative antioxidant activity and HPLC profiles of some selected Korean thistles. Arch Pharm Res 31(1): 28-33 

    원문보기 상세보기 crossref

  4. Jeong HC, Shim YS, Rhee YK, Choi SY, Hong HD, Chung J, Han MJ, Cho CW (2013) Quantification of marker compounds in Cirsium setidens Nakai by HPLC-DAD. Food Sci Biotechnol 22(6): 1481-1486 

    원문보기 상세보기 crossref

  5. Jordon-Thanden IE, Louda SM (2001) Chemistry of Cirsium and Carduus; a role in ecological risk assessment for biological control of weeds? Biochem Syst Ecol 31(12): 1353-1396 

  6. Jung HA, Jin SE, Min BS, Kim BW, Choi JS (2012) Anti-inflammatory activity of Korean thistle Cirsium maackii and its major flavonoid, luteolin 5-O-glucoside. Food Chem Toxicol 50(6): 2171-2179 

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  7. Jung HA, Kim YS, Choi JS (2009) Quantitative HPLC analysis of two key flavonoids and inhibitory activities against aldose reductase from different parts of the Korean thistle, Cirsium maackii. Food Chem Toxicol 47(11): 2790-2797 

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  8. Kim EY, Jho HK, Kim EI, Rhyu MR (2008) Cirsium japonicum elicits endothelium-dependent relaxation via histamine H(1)-receptor in rat thoracic aorta. J Ethnopharmacol 116(2): 223-227 

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  9. Kim SJ, Kim GH (2003) Identification for flavones in different parts of Cirsium japonicum. J Food Sci Nutr 8(4): 330-335 

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  10. Ku KL, Tsai CT, Chang WM, Shen ML, Wu CT, Liao HF (2008) Hepatoprotective effect of Cirsium arisanense kitamura in tacrine-treated hepatoma Hep 3B cells and C57BL mice. Am J Chin Med 36(2): 355-368 

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  11. Lee BL, Kwan JH, Zee OP, Yoo SJ (1994) Flavonoids from Cirsium rhinoceros. Arch Pharm Res 17(4): 273-277 

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  12. Lee BW, Kwon CH, Cho OR, Lee KC, Choi SU, Baek NI, Lee KR (2002) Phytochemical constituents of Cirsium setidens Nakai and their cytotoxicity against human cancer cell lines. Arch Pham Res 25(5): 628-635 

    원문보기 상세보기 crossref

  13. Lim H, Son KH, Chang HW, Bae KH, Kang SS, Kim HP (2008) Anti-inflammatory activity of pectolinarigenin and pectolinarin isolated form Cirsium chanroenicum. Biol Pharm Bull 31(11): 2063-2067 

    상세보기 crossref

  14. Liu S, Lou X, Li D, Zhang J, Qiu DL, Liu W, She L, Yang Z (2006) Tumor inhibition and improved immunity in mice treated with flavone from Cirsium japonicum DC. Int Immunopharmacol 6(9): 1387-1393 

    상세보기 crossref

  15. Liu S, Zhang J, Li D, Liu W, Luo X, Zhang R, Li L, Zhao J (2007) Anticancer activity and quantitative analysis of flavone of Cirsium japonicum DC. Nat Prod Res 21(10): 915-922 

    상세보기 crossref

  16. Martinez-Vazquez M, Ramirez Apan TO, Lastra AL, Bye R (1998) A comparative study of the analgesic and anti-inflammatory activities of pectolinarin isolated from Cirsium subcoriaceum and linarin isolated from Buddleia cordata. Planta Med 64(2): 134-137 

    상세보기 crossref

  17. Nazaruk J, Jakoniuk P (2005) Flavonoid composition and antimicrobial activity of Cirsium rivulare (Jacq.) All. flowers. J Ethnopharmacol 102(2): 208-212 

    상세보기 crossref

  18. Park JC, Hur JM, Park JG, Kim SC, Park JR, Choi SH, Choi JW (2004) Effects of methanol extract of Cirsium japonicum var. ussuriense and its principle, hispidulin-7-O-neohesperidoside on hepatic alcohol-metabolizing enzymes and lipid peroxidation in ethanol-treated rats. Phytother Res 18(1): 19-24 

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  19. Park MJ, Choi JK, Kakishima M, Shin HD (2011) First report of rust disease caused by Puccinia nishidana on Cirsium setidens. Plant Pathol J 27(3): 297 

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  20. Perez GR, Ramirez LM, Vargas SR (2001) Effect of Cirsium pascuarense on blood glucose levels of normoglycaemic and alloxan-diabetic mice. Phytother Res 15(6): 552-554 

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  21. Simoes LR, Maciel GM, Brandao GC, Filho JD, Oliveifa AB, Castilho RO (2013) Chemical constituents of Distictella elongate (Vahl) Urb. (Biognoniaceae). Ann Braz Acad Sci 85(3): 873-879 

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  22. Sun Q, Chang L, Ren Y, Cao L, Sun Y, Du Y, Shi X, Wang Q, Zhang L (2012) Simultaneous analysis of 11 main active components in Cirsium setosum based on HPLC-ESI-MS/MS and combined with statistical methods. J Sep Sci 35(21): 2897-2907 

    상세보기 crossref

  23. Yim SH, Kim HJ, Lee IS (2003) A polyacetylene and flavonoids from Cirsium rhinoceros. Arch Pharm Res 26(2): 128-131 

    원문보기 상세보기 crossref

  24. Yoo YM, Nam JH, Kim MY, Choi JW, Park HJ (2008) Pectolinarin and pectolinarigenin of Cirsium setidens prevent the hepatic injury in rats caused by D-galactosamine via an antioxidant mechanism. Biol Pharm Bull 31(4): 760-764 

    상세보기 crossref

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