[논문]Paramagnetic Zn(1-x)MnxO (0.00≤x≤0.06) Nanoparticles Prepared by The Coprecipitation Method

Harsono, Heru; Wardana, I Nyoman Gede; Sonief, Achmad As'ad; Darminto, Darminto

doi:10.4313/teem.2017.18.1.46

[국내논문] Paramagnetic Zn(1-x)MnxO (0.00≤x≤0.06) Nanoparticles Prepared by The Coprecipitation Method 원문보기

Transactions on electrical and electronic materials, v.18 no.1, 2017년, pp.46 - 50

Harsono, Heru (Department of Mechanical Engineering, Faculty of Engineering and Department of Physics, Faculty of Mathematics and Natural Sciences, Universitas Brawijaya) , Wardana, I Nyoman Gede (Department of Mechanical Engineering, Faculty of Engineering, Universitas Brawijaya) , Sonief, Achmad As'ad (Department of Mechanical Engineering, Faculty of Engineering, Universitas Brawijaya) , Darminto, Darminto (Department of Physics, Faculty of Mathematics and Natural Sciences, Institut Teknologi Sepuluh Nopember)

Abstract ▼ AI-Helper

The Zn1-xMnxO ($0.00{\leq}x{\leq}0.06$) samples have been synthesized in the form of powder by the coprecipitation method at low temperature using $Zn(CH_3COO)_2$. $2H_2O$ and $Mn(CH_3COO)_2$. $4H_2O$ powders, as well as HCl and $NH_4OH$ solutions as starting materials. Characterization was conducted using XRD, TEM, XRF, FTIR and VSM. The result shows that the $Zn_{(1-x)}Mn_xO$ ($0.00{\leq}x{\leq}0.06$) nanoparticles have the wurtzite phase with a hexagonal structure and particle sizes ranging from 17.48 to 118.83 nm. In a qualitative analysis of XRF, the peaks that confirm the existence of the manganese element in Mn-doped ZnO samples were observed. Meanwhile, FTIR test result shows that there are peaks at around $500cm^{-1}$ and $400cm^{-1}$ in the FTIR spectra for Mn doped ZnO samples which clearly reveal the existence of the (Zn, Mn)-O strain mode. The (Zn, Mn)-O absorption peak positions have shifted to a lower wave number with increasing Mn doping content. The peak intensity is also lower if compared to that of the ZnO sample without doping. From the VSM test, it is shown that $Zn_{(1-x)}Mn_xO$ ($0.00{\leq}x{\leq}0.06$) nanoparticles are all paramagnetic having monotonically increased susceptibility as increasing Mn content.

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제안 방법

In this article, we report the successful synthesis of Zn(1-x)MnxO (0.00≤x≤0.06) nanopowders employing the coprecipitation method.
Transmission electron microscopy (TEM, JEOL-JEM 1400) and the spectrum of the X-Ray Fluorescence (XRF, PANalytical MiniPA14) from the Zn(1-x)MnxO (0.00≤x≤0.06) samples were employed to study the morphological characteristics and elemental content.
Analysis of the diffraction pattern was undertaken with the Rietveld refinement method using the Rietica program to explore the crystal structure of the Zn(1-x)MnxO (0.00≤x≤0.06) sample.
To determine the magnetic properties of Zn(1-x)MnxO (0.00≤x≤0.06) nanoparticles, characterization was conducted by using a VSM (vibrating sample magnetometer) at room temperature.

대상 데이터

4H2O (Aldrich Chemistry,≥99%), 37% HCl (Merck), and NH4OH 25% (Merck).
The chemicals used were zinc acetate dihydrate Zn(CH₃COO)₂. 2H₂O (Merck,≥99%), manganese (II) acetate tetrahydrate Mn(CH₃COO)₂.

데이터처리

Phase identification analysis was conducted with the X’Pert High Score Plus program.

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