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NTIS 바로가기Journal of carbohydrate chemistry, v.21 no.6, 2002년, pp.513 - 520
Moe, St⊘rker (Department of Chemical Engineering, Norwegian University of Science and Technology, Sem Sæ) , Holen †, Anne (lands vei 4, NO-7491, Trondheim, Norway) , Schult ††, Tove (Department of Chemical Engineering, Norwegian University of Science and Technology, Sem Sæ)
Mild ozonation of cellobiose in acetic acid almost exclusively favors oxidation of the reducing end, thus yielding 4-O-β-d-glucopyranosyl-d-gluconic acid (“cellobionic acid”). This compound can be quantitatively separated from the substrate by preparative HPLC using acetonitrile/phosphate buffer on an aminopropyl silica column. The product was identified using one and two dimensional NMR techniques. 13 C and 1 H NMR chemical shifts are reported.
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