[논문]HPLC-DAD-MS를 이용한 천연염색 면직물의 천연색소 지표성분에 대한 분석

이원경; 김종훈; 김문정; 박윤철; 이범훈

doi:10.5764/tcf.2020.32.4.255

HPLC-DAD-MS를 이용한 천연염색 면직물의 천연색소 지표성분에 대한 분석
Analysis of Natural Pigment Indicator Components of Natural Dyed Cotton Fabrics Using HPLC-DAD-MS 원문보기

韓國染色加工學會誌 = Textile coloration and finishing, v.32 no.4, 2020년, pp.255 - 264

이원경 (한국섬유소재연구원) , 김종훈 (한국섬유소재연구원) , 김문정 (한국섬유소재연구원) , 박윤철 (한국생산기술연구원) , 이범훈 (신한대학교 섬유소재공학과)

Abstract ▼ AI-Helper

With the development of synthetic dyes, excellent dyeing properties and massive production became possible. On the other hand, natural dyeing technology has gradually disappeared. However, the international environmental and human safety requirements of the apparel and textile industry are increasing, and there is a growing interest in safer and more environmentally friendly products. Accordingly, the public's interest in natural dyeing is increasing. To meet these demands, it is first necessary to clarify the stages of production and distribution of natural dyes. It is necessary to evaluate whether the product is a natural dye product and study the suitability of the natural dye product through qualitative and quantitative assessment of the indicator components of the natural dye. Typical of three natural dyes did qualitative and quantitative analysis by HPLC-DAD and HPLC-MS. Products dyed using natural dye three products were analyzed, and the presence or absence of detection of each indicator components was confirmed to confirm whether the product was dyed using natural dyes.

주제어

표/그림 (14)

표 Table 1. Natural dyes in this experimental
표 Table 2. Natural dyeing process
표 Table 3. Reference standard in this study
표 Table 4. Analytical condition of HPLC-DAD
표 Table 5. Analytical conditions of HPLC-MS
그림 Figure 1. HPLC Chromatogram, DAD UV-spectra and MS-data of rubia natural dye.
그림 Figure 2. Calibration curve of rubia natural dye.
그림 Figure 3. HPLC Chromatogram, DAD UV-spectra and MS-data of insect natural dye.
그림 Figure 4. Calibration curve of insect natural dye.
그림 Figure 5. HPLC Chromatogram, DAD UV-spectra and MS-data of indigo natural dye.
그림 Figure 6. Calibration curve of indigo natural dye.
그림 Figure 7. HPLC Chromatogram of extract from dyed with rubia on cotton fabric.
그림 Figure 8. HPLC Chromatogram of extract from dyed with insect on cotton fabric.
그림 Figure 9. HPLC Chromatogram of extract from dyed with indigo on cotton fabric.

참고문헌 (13)

M. L. Gulrajani, Present Status of Natural Dyes, Indian Journal of Fiber and Textile Research, 26, 191(2001).
D. D. Santis and M. Moresi, Production of Alizarin Extracts from Rubia Tinctorum and Assessment of their Dyeing Properties, Industrial Crops and Products, 26, 151(2007).

상세보기
M. K. Kim, Study on Natural Polygoum Tinctoria Dyeing of Sustainable Eco-friendly Cellulose Fabric and its Application, Ph.D. Thesis, Ehwa Women's University, 2012.
S. H. Youn, The Prospect of Industrial Value and Potential of Natural Dyeing, Dyeing and Finishing, 4, 47(2009).
https://www.betalabservices.com/natural-products/curcuminanalysis.html, 2020.11.10.
D. Hemen and L. Ledwani, A Review on Anthraquinones Isolated from Cassia Species and their Applications, Indian Journal of Natural Products and Resources, 3(3), 291(2012).
S. H. Youn and Y. J. Lim, Stabilization of Natural Dyes and Establishment of Reproducibility of Dyeing, Fiber Technology and Industry, 9(2), 162(2005).
J. E. Oh and C. S. Ahn, Analysis of the Pigment Contents of Commercial Indigo Powders and their Effect on the Color and the Antimicrobial Function of Dyed Cotton Fabrics, Journal of the Korean Society of Clothing and Textiles, 37(1), 17(2013).

원문보기 상세보기
J. Y. Lim and J. D. Jang, Dye Extraction and Silk Dyeing of Rubia Cordifolia using Solvent, Journal of the Korean Society of Clothing and Textiles, 37(4), 506(2013).

원문보기 상세보기
M. R. S. Fuh and H. J. Lin, Analysis of Rhubarb by Liquid Chromatography Electrospray-mass Spectrometry, Tamkang Journal of Science and Engineering, 6(1), 31(2003).

상세보기
C. S. Ahn, X. Zeng, and S. K. Obendorf, Simultaneous Analysis of the Coloring Compounds in Indigo, Phellodendron bark, and Madder Dye Using HPLC-DAD-MS, Journal of the Korean Society of Clothing and Textiles, 37(6), 827(2013).

원문보기 상세보기
C. S. Ahn and S. K. Obendorf, Separation of Chromophoric Substance from Madder Plant under Different Extraction and Analytical Conditions, Journal of the Korean Society of Clothing and Textiles, 27(11), 1350(2003).
E. M. Lee, D. K. Oh, H. J. Yoon, and J. H. Kim, A Study for the Conformity Assessment on the Natural Dye by HPLC(1), Fashion and Text. Res. J., 20(6), 2287(2018).

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