[논문]New Analysis of Electrochemical Impedance Spectroscopy for Lithium-ion Batteries

Osaka, Tetsuya; Nara, Hiroki; Mukoyama, Daikichi; Yokoshima, Tokihiko

doi:10.5229/jecst.2013.4.4.157

[국내논문] New Analysis of Electrochemical Impedance Spectroscopy for Lithium-ion Batteries 원문보기

Journal of electrochemical science and technology, v.4 no.4, 2013년, pp.157 - 162

Osaka, Tetsuya (Faculty of Science and Engineering, Waseda University) , Nara, Hiroki (Faculty of Science and Engineering, Waseda University) , Mukoyama, Daikichi (Faculty of Science and Engineering, Waseda University) , Yokoshima, Tokihiko (Faculty of Science and Engineering, Waseda University)

Abstract ▼ AI-Helper

First of all, we express our deepest sympathies for the passing of Professor Su-Moon Park. In the present paper, an electrochemical impedance spectroscopy (EIS), which Professor Su-Moon Park also used frequently for the investigation of electroconducting polymer, is introduced as a recent evaluation tool for a commercially available lithium-ion battery (LIB). The paper surveys how to design equivalent circuits while explaining physical and chemical phenomena in the LIB and how to get more accurate impedance spectra with varying the measuring temperatures. Additionally, a square current EIS (SC-EIS) technique, which we have suggested, is introduced for the larger LIB system as a promising technique for the future.

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제안 방법

Using the technique of Fourier transform in ref,^26,27 SC-EIS was carried out using the square current input. Optimization of the measuring condition(i.e. frequency of square current), DC-offset, amplitude from 0 to the peak, and sampling frequency, enabled the measurement of the impedance of the LIB cell by SC-EIS as well as by EIS using a conventional FRA and potentiostat system. Specifically, there was a good accordance between Nyquist plots obtained by SC-EIS on an LIB cell and those obtained by EIS using a conventional FRA and potentiostat system with the error of each plot being less than 3% in the range of 1 kHz - 1 Hz.
In all the spectra obtained in the work, three domains were visually separated into a region of loci in the 1st quadrant, regions of superposition of arcs or semicircles, and loci of increase in the imaginary components, with frequency regions of 100-10 kHz, 10 kHz to 100 mHz, 100-0.1 mHz, respectively. Fig.

대상 데이터

A commercially-available laminated LIB was used in the work. Using the technique of Fourier transform in ref,^26,27 SC-EIS was carried out using the square current input.

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