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NTIS 바로가기한국식품과학회지 = Korean journal of food science and technology, v.44 no.6, 2012년, pp.658 - 665
최은정 (서울시보건환경연구원) , 강성태 (서울과학기술대학교 식품공학과) , 정소영 (서울시보건환경연구원) , 신재민 (서울시보건환경연구원) , 장민수 (서울시보건환경연구원) , 이상미 (서울시보건환경연구원) , 김정헌 (서울시보건환경연구원) , 채영주 (서울시보건환경연구원)
A survey of zearalenone contamination was conducted on cereal-based products by using an immunoaffinity column with LC-MS/MS. The calibration curve showed good lineality, with correlation coefficients (
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핵심어 | 질문 | 논문에서 추출한 답변 |
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Fusarium속 곰팡이 독소인 제랄레논은 인체에 어떤 영향을 주는가? | 비스테로이드성 에스트로겐으로 알려진 제랄레논은 국제암연구소(International Agency for Research on Cancer, IARC)에서 인체발암성이 없는 물질(Grop 3)로 분류하고 있지만, 유산, 불임등 생식에 관련된 독성을 유발하며, 내분비계 장애물질로서 호르몬계 이상을 초래한다(3). | |
제랄레논은 어떤 독소인가? | 제랄레논(Zearalenone)은 Fusarium graminearum, Fusarium moniliforme 등의 곰팡이에 의해 생성 되는 Fusarium속 곰팡이 독소로서, 옥수수, 보리, 밀과 같은 농산물 중 탄수화물 함량이 높은 작물에서 주로 발생된다(1). Resorcyclic acid lactone으로서 화학적으로 6-(10-hydroxy-6-oxo-trance-1-undecenyl)-β-resorcyclic acid lactone으로 표시 할 수 있다. | |
제랄레논은 어느 작물에서 주로 발생하는가? | 제랄레논(Zearalenone)은 Fusarium graminearum, Fusarium moniliforme 등의 곰팡이에 의해 생성 되는 Fusarium속 곰팡이 독소로서, 옥수수, 보리, 밀과 같은 농산물 중 탄수화물 함량이 높은 작물에서 주로 발생된다(1). Resorcyclic acid lactone으로서 화학적으로 6-(10-hydroxy-6-oxo-trance-1-undecenyl)-β-resorcyclic acid lactone으로 표시 할 수 있다. |
Monstrom MS. Zearalenone. Vol. 77, pp. 977-982. In: Veterinary Toxicology, Gupta RC. Academic Press, Waltham, MA, USA (2007)
EFSA (European Food Safety Authority). Opinion of the scientific panel on contaminants in food chain on a request from the commission related to zearalenone as undesirable substances in animal feed. EFSA J. 89: 1-35 (2004)
IARC. Some naturally occurring substances: food items and constituents. heterocyclic aromatic amines and mycotoxins. IARC monographs on the evaluation of carcinogenic risks to humans 56: 397-444 (1993)
Martins ML, Martins HM. Influence of water activity, temperature and incubation time on the simultaneous production of deoxynivalenol and zearalenone in corn (Zea mays) by Fusarium graminearum. Food Chem. 79: 315-318 (2002)
Jang MR, Lee CH, Lee HJ, Kim JY, Son SH, Shin CS, Kim SH, Kim DB. A survey of zearalenone in beans using high performance liquid chromatography-fluorescence detector (HPLC-FLD) and ultra performance liquid chromatography tandem mass spectometry (LC-MS/MS). Korean J. Food Sci. Technol. 40: 354-359 (2008)
Romagnoli B, Ferrari M, Bergamini C. Simultaneous determination of deoxynivalenol, zearalenone, T-2, and HT-2 toxins in breakfast cereals and baby food by high-performance liquid chromatography and tandem mass spectometry. J. Mass Spectrom. 45: 1075-1080 (2010)
Senyuva HZ, Gilbert J. Immunoaffinity column clean-up techniques in food analysis: A review. J. Chromatogr. B 878: 115-132 (2010)
Shephard GS, Berthiller F, Burdaspal P, Crews C, Jonker MA, Krska R, Macdonald S, Malone B, Maragos C, Sabino M, Solfrizzo M, Egmond HPV, Whitaker TB. Developments in Mycotoxin analysis: An update for 2009-2010. World Mycotoxin J. 4: 3-28 (2011)
Rahmani A, Jinap S, Soleimany F. Qualitative and quantitative analysis of mycotoxins. Compr. Rev. Food Sci. F. 8: 202-251 (2009)
Lindner W, Zollner P, Jodlbauer J. Determination of zearalenone in grains by high-performance liquid chromatography-tandem mass spectrometry after solid-phase extraction with RP-18 columns or immunoaffinity columns. J. Chromatogr. A 858: 167-174 (1999)
Schollenberger M, Muller HM, Rufle M, Suchy S, Planck S, Drochner W. Survey of Fusarium toxins in foodstuffs of plant origin marketed in germany. Int. J. Food Microbiol. 97: 317-326 (2005)
Jang MR, Lee CH, Choi IS, Shin CS, Kim JH, Jang YM, Kim DS, Ahn DH. Analysis of zearalenone contamination in cerealbased products using high performance liquid chromatographyfluorescence detector and ultra performance liquld chromatography- tandem mass spectometry. Korean J. Food Sci. Technol. 43: 224-229 (2011)
Jinap S, Soleimany F, Abas F. Determination of mycotoxins in cereals by liquid chromatography tandem mass spectrometry. Food Chem. 130: 1055-1060 (2012)
ISO. Guide to the Expression of Uncertainty in Measurements. International Organization (ISO), Geneva, Switzerland (1993)
Kim YJ, Kim HW. Estimation of measurement uncertainty in vitamin c analysis from vegetable and fruit juice. Korean J. Food Sci. Technol. 35: 1053-1059 (2003)
EURACHEM, Quantifying uncertainty in analytical measurement, 2nd, EURACHEM, London, UK (2000)
KOLAS, Guideline for quantifying and expressing the uncertainty in measurement results. Korea Laboratory Accereditation Schem, Daejon, Korea (2000)
EFSA (European Food Safety Authority). Zearalenone in food, scientific opinion of the panel on contaminations in the food chain. EFSA J. 2197: 1-124 (2011)
Moreno-Bondi MC, Urraca JL, Marazuela MD, Moreno. Analysis for zearalenone and ${\alpha}$ -zearalenol in cereals and swine feed using accelerated solvent extraction and liquid chromatography with fluorescence detection. Anal. Chim. Acta 524: 175-183 (2004)
Mateo JJ, Mateo R, Hinojo MJ, Llorens A, Jimenez M. Liquid chromatographic determination of toxigenic secondary metabolites produced by Fusarium strains. J. Chromatogr. A 955: 245-256 (2002)
Soler C, Rubert J, Manes J. Application of an HPLC-MS/MS method for mycotoxin analysis in commercial baby foods. Food Chem. 133: 176-183 (2012)
EU. Report on the relationship between analytical results, measurement uncertainty, recovery factors and the provisions of EU food and feed legislation, with particular reference to community legislation concerning. Available at: http://ec.europa.eu/food/food/chemicalsafety/contaminants/sampling_en.print.htm. Jan. 9, 2010.
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