[논문]Ti3C2TX MXene 기반 유연 전극 기술 개발 동향

최수빈; 미나자간싱; 김종웅

doi:10.6117/kmeps.2022.29.1.017

[국내논문] Ti3C2TX MXene 기반 유연 전극 기술 개발 동향
Technical Trends of Ti3C2TX MXene-based Flexible Electrodes 원문보기

마이크로전자 및 패키징 학회지 = Journal of the Microelectronics and Packaging Society, v.29 no.1, 2022년, pp.17 - 33

최수빈 (전북대학교 신소재공학부) , 미나자간싱 (전북대학교 신소재공학부) , 김종웅 (전북대학교 신소재공학부)

초록
AI-Helper

2011년 Naguib 그룹에서 처음 보고한 Ti₃C₂T_X MXene은 우수한 친수성, 전기 전도성 및 기계적/화학적 안정성으로 인해 큰 주목을 받고 있다. 특히, MXene은 수 나노미터 두께를 지닌 2차원 물질이므로 유연성을 확보하기에 용이하기 때문에 스마트 센서, 에너지 하베스팅/저장 시스템, 수퍼커패시터 및 전자기 차폐 시스템 등 여러 분야에 적용하고자 한 연구 결과가 많이 보고되었다. 본 논문에서는 Ti₃C₂T_X MXene의 다양한 합성 공정 및 특성에 대해 간략히 소개한 후, Ti₃C₂T_X MXene을 유연 전극 물질로 이용한 최근 연구 결과를 알아보고자 한다.

Abstract ▼ AI-Helper

Ti3C2TX MXene, first reported by Naguib et al. in 2011, has attracted tremendous attention due to its excellent hydrophilicity, electrical conductivity, and mechanical/chemical stability. Since MXene is a two-dimensional material with a thickness of few nanometers, which ensure its flexibility. In last few years, due to these properties many researchers used Ti3C2TX MXene into various fields such as flexible smart sensors, energy harvesting/storage devices, supercapacitors and electromagnetic interference shielding systems. In this review article, we have briefly discussed the various synthesis processes and characteristics of Ti3C2TX MXene. Moreover, we reviewed the latest development of Ti3C2TX MXene as flexible electrode material to be used into different applications.

Keyword

표/그림 (13)

그림 Fig. 1. Schematic illustration of SF@MXene bicomposite film-based flexible pressure sensor.⁴⁹⁾
49)" alt="Fig. 2. Applications of the SF@Mxene film-based flexible pressure sensor for the detection of various physiological human motions. (a) Overview of sensing applications and locations. (b) Measurement of blood pressure using device on wrist of the volunteer. (c) Single pulse waveform extracted from (b). (d) Photograph of the SF@Mxene film-based flexible pressure sensor attached onto the throat. (e) The corresponding ΔI/I0 of swallowing. (f) the relative current variation-time curve of the SF@Mxene film-based flexible sensor in response to these pronunciations of "silk" and "MXene". (g) Current variation of the bending sensor under a series of increasing step bending angle from 30 to 90◦. Inset is the photograph of the bending device. (h) Response of the SF@Mxene film-based flexible pressure sensor in monitoring finger bending. Inset is the photographs of finger motions. (i) Real-time monitoring of the SF@Mxene film-based flexible pressure sensor for finger bending. Inset is the photographs of the finger state.⁴⁹⁾" onerror="this.src='/images/noimg.png'" class="objectfit" /> 그림 Fig. 2. Applications of the SF@Mxene film-based flexible pressure sensor for the detection of various physiological human motions. (a) Overview of sensing applications and locations. (b) Measurement of blood pressure using device on wrist of the volunteer. (c) Single pulse waveform extracted from (b). (d) Photograph of the SF@Mxene film-based flexible pressure sensor attached onto the throat. (e) The corresponding ΔI/I0 of swallowing. (f) the relative current variation-time curve of the SF@Mxene film-based flexible sensor in response to these pronunciations of "silk" and "MXene". (g) Current variation of the bending sensor under a series of increasing step bending angle from 30 to 90◦. Inset is the photograph of the bending device. (h) Response of the SF@Mxene film-based flexible pressure sensor in monitoring finger bending. Inset is the photographs of finger motions. (i) Real-time monitoring of the SF@Mxene film-based flexible pressure sensor for finger bending. Inset is the photographs of the finger state.⁴⁹⁾
그림 Fig. 3. (a) Schematic illustration of the fabrication of a conductive, anti-freezing, and self-healing MNOH. SEM images of b) delaminated MXene sheet, and (c,d) the freeze-dried MNH.⁵⁰⁾
그림 Fig. 4. Strain sensing characteristics of the MC@p-NWF based strain sensor. Cyclic strain sensing behaviors of the strain sensor under different (a) strain levels and (b) tensile rates. (c) I–V curves of the strain sensor under different strains. (d) Response and recovery times of the strain sensor under instantaneous tension (3(1/4) 1%, 500mm min.¹⁾ (e) Cycling stability of the strain sensor over 1000 cycles in 10% strain at a tensile rate of 10 mm/min. (f) Photographs of an LED connected with the strain sensor, showing light intensity variation under external stretching and release. (g) Comparison of the maximum working range and GF of our strain sensor with those reported in previous studies.⁵¹⁾
그림 Fig. 5. (a) Voltage profiles of Zn plating/stripping process with bare Zn anode (black) and Ti₃C₂T_x MXene@Zn anode (red) at a current density of 1 mA cm⁻² and an areal capacity of 1 mAh cm⁻². Enlarged voltage profiles at (b) the first six cycles and (c) from 78th to 84th cycles. SEM im age of (d) bare Zn and (e) Ti₃C₂T_x MXene@Zn anode after being cycled.⁵²⁾
그림 Fig. 6. (a) The charge–discharge voltage profiles and (b) cycling performance of the MXene@CNF/Li||LFP and Cu/Li||LFP full cell at 0.2 C. (c) Rate performance of the MXene@CNF/Li||LFP and Cu/Li full cell from 0.1 C to 2 C. (d) Schematic of a possible fully flexible MXene@CNF/Li||LFP@CNF battery. (e) The charge-discharge voltage profiles and (f) the cycling performance of the MXene@CNF/Li||LFP@CNF full cell at 0.2 C.⁵³⁾
그림 Fig. 7. Electrochemical performances of the MXene electrodes: (a) cycle performance at 50 mA g⁻¹ and (b) rate property of the stacked MXene film and the 3D porous MXene foams; (c) long-term cycle stability of the p-MXene-71 electrode; (d,e) Nyquist plots with the equivalent circuit before cycle and after 300 cycles.⁵⁴⁾
그림 Fig. 8. Durability of the AgNW film and MA film. Changes in sheet resistance for the A164 film and MA20/164 film by exposing in (a) air at room temperature for 70 days and (b) a sulfur-vapor environment at 100℃ for 40 min. Insets are SEM images of a neat AgNW film and MA film after being exposed to different environments. (c) EMI shielding performances of an A326 film and MA20/184 film before and after exposure to air and sulfur vapor. Resistance changes of A164, MA20/164, and ITO films upon (d) different bending radii (outcurve) and (e) cyclic bending tests with a radius of 1.3 mm. (f) long-term stability of EMI SE for an MA20/205 film after 3000 bending cycles at a radius of 1.3 mm.⁵⁵⁾
그림 Fig. 10. Structure and properties of the MXene/CNF hybrid aerogels with various CNF contents. Microstructures of the MXene/CNF hybrid aerogels with (a) 17 wt.% and (b) pure MXene aerogels, at densities of 4 mg cm^–3. (c) Optical images of the MXene-based hybrid aerogels, showing large-area MXene/CNF aerogels (12×6 cm²) with various CNF contents (from top to bottom, corresponding to the pure CNF aerogels, the MXene/CNF with 50 wt.% CNF, and MXene/CNF with 17 wt.% CNF) at a density of 4 mg cm^–3, and an image demonstrating the flexible performance of the MXene/CNF aerogels with 17 wt.% CNF. (d) Electrical conductivity and compressive modulus of the MXene-based aerogels (4 mg cm^–3) with various CNF contents. (e) EMI SE in the X-band and (f) shielding performance at 10 GHz of the MXene-based hybrid aerogels (4.0 mg cm^–3) with various CNF contents.⁵⁷⁾
그림 Fig. 9. (a) Plot of conductivity of M-textile versus content of PPy/MXene hybrid in textile with different dip-coating cycle numbers. (b) normalized relative resistance changes of M-textile and its silicone-coated counterpart during bending and torsion tests. (c) normalized relative resistance variation of silicone-coated M-textile to show its long-term durability. (d) plots of EMI SE versus frequency for M-textiles with different conductivities (0.43 mm). (e) effect of thickness on EMI SE for M-textiles (1000 S m⁻¹). (f) plots of EMI SE versus frequency for silicone-coated M-textiles with different conductivities (0.45 mm).⁵⁶⁾
그림 Fig. 11. The electrical characterization of the TENG. (a) The open-circuit voltage (V_oc) waveforms of the TENG for various wt. % of MXene in PVDF. (b) The shortcircuit current (I_sc) waveforms of the TENG for various wt. % of MXene in PVDF. (c) Charge waveforms of TENG for different wt. % of MXene in PVDF. Measured (d) V_oc, (e) Isc, and (f) charge waveforms of TENG at varying input frequencies. Measured (g) V_oc, (h) I_sc, and (i) charge waveforms of TENG at varying vertical impact force at 1 Hz frequency.⁵⁸⁾
그림 Fig. 12. Operating principles and output performance of the MH-TENG. (a) A schematic structure of the MH-TENG. (b) A schematic working principle of the single-electrode mode MH-TENG for energy harvesting. (c) The triboelectric mechanism based on microchannels of the MXene/PVA hydrogel. (d) Open-circuit voltage, (e) short-circuit current, and (f) transferred charge amount of the MH-TENGs for different doping concentrations of MXene nanosheets. (g) Resistance of the MXene/PVA hydrogel with different MXene doping concentrations.⁵⁹⁾
그림 Fig 13. (a) Schematic illustration of the working mechanism for single-electrode mode MAMP-TENG. (b) Real-time output voltage and output current signals of hand tapping TENG. (c) The output voltage of a 3.3 μF capacitor charged by the MAMP-TENG with hand tapping. (d) Photograph of 40 LEDs lighted by MAMP-TENG. (e) Output voltage of MAMP-TENG under different strains. (f) Output voltage and (g) output current at different frequencies. (h) Output voltage of MAMP-TENG in response to different fabrics.⁶⁰⁾

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Q. Zhao, Q. Zhu, J. Miao, P. Zhang, P. Wan, L. He and B. Xu, "Flexible 3D Porous MXene Foam for High-Performance Lithium-Ion Batteries", Small, 15(51), 1904293-1904302 (2019).

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W. Chen, L. X. Liu, H. B. Zhang and Z. Z. Yu, "Flexible, Transparent, and Conductive Ti 3 C 2 T x MXene-Silver Nanowire Films with Smart Acoustic Sensitivity for High-Performance Electromagnetic Interference Shielding", ACS Nano, 14(12), 16643-16653 (2020).
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표제어: PCR

동의어: Packet Collision Rate

용어 설명 출처 목록 (6)

용어 설명: PCR은 세균 특이성이 있는 primer를 이용하여 적은 수의 세균이 있을지라도 쉽게 검출할 수 있는 유용한 방법이며, 이를 이용하여 구강 내 치면세균막이나 타액에서 직접 세균을 검출할 수 있게 되었다[8].

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